((S)-1-[1,3]Dioxolan-2-yl-2-phenyl-ethyl)-(2-trimethylsilanylmethyl-allyl)-carbamic acid methyl ester

Base Information

Chemical Name:((S)-1-[1,3]Dioxolan-2-yl-2-phenyl-ethyl)-(2-trimethylsilanylmethyl-allyl)-carbamic acid methyl ester
CAS No.:114724-30-0
Molecular Formula:C₂₀H₃₁NO₄Si
Molecular Weight:377.556
Hs Code.:

Synonyms:((S)-1-[1,3]Dioxolan-2-yl-2-phenyl-ethyl)-(2-trimethylsilanylmethyl-allyl)-carbamic acid methyl ester

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Chemical Property of ((S)-1-[1,3]Dioxolan-2-yl-2-phenyl-ethyl)-(2-trimethylsilanylmethyl-allyl)-carbamic acid methyl ester

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Technology Process of ((S)-1-[1,3]Dioxolan-2-yl-2-phenyl-ethyl)-(2-trimethylsilanylmethyl-allyl)-carbamic acid methyl ester

There total 7 articles about ((S)-1-[1,3]Dioxolan-2-yl-2-phenyl-ethyl)-(2-trimethylsilanylmethyl-allyl)-carbamic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3182-95-4
L-Phenylalaninol

: 114724-30-0
((S)-1-[1,3]Dioxolan-2-yl-2-phenyl-ethyl)-(2-trimethylsilanylmethyl-allyl)-carbamic acid methyl ester

Guidance literature:: Multi-step reaction with 7 steps

1: 95 percent / Et₃N / CH₂Cl₂

2: 93 percent / (COCl)2-Me₂SO, Et₃N / CH₂Cl₂ / -78 °C

3: p-toluenesulfonic acid

4: p-toluenesulfonic acid

5: H₂ / Pd/C

6: i-Pr₂NEt / CH₂Cl₂ / Ambient temperature

7: Et₃N / CH₂Cl₂

With oxalyl dichloride; hydrogen; toluene-4-sulfonic acid; dimethyl sulfoxide; triethylamine; N-ethyl-N,N-diisopropylamine; palladium on activated charcoal; In dichloromethane;
DOI:10.3987/R-1987-11-2805

Reference yield:

: 59830-60-3
benzyl (1S)-(1-formyl-2-phenylethyl)carbamate

: 114724-30-0
((S)-1-[1,3]Dioxolan-2-yl-2-phenyl-ethyl)-(2-trimethylsilanylmethyl-allyl)-carbamic acid methyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: p-toluenesulfonic acid

2: p-toluenesulfonic acid

3: H₂ / Pd/C

4: i-Pr₂NEt / CH₂Cl₂ / Ambient temperature

5: Et₃N / CH₂Cl₂

With hydrogen; toluene-4-sulfonic acid; triethylamine; N-ethyl-N,N-diisopropylamine; palladium on activated charcoal; In dichloromethane;
DOI:10.3987/R-1987-11-2805

Reference yield:

: 6372-14-1
N-((benzyloxy)carbonyl)-L-phenylalaninol

: 114724-30-0
((S)-1-[1,3]Dioxolan-2-yl-2-phenyl-ethyl)-(2-trimethylsilanylmethyl-allyl)-carbamic acid methyl ester

Guidance literature:: Multi-step reaction with 6 steps

1: 93 percent / (COCl)2-Me₂SO, Et₃N / CH₂Cl₂ / -78 °C

2: p-toluenesulfonic acid

3: p-toluenesulfonic acid

4: H₂ / Pd/C

5: i-Pr₂NEt / CH₂Cl₂ / Ambient temperature

6: Et₃N / CH₂Cl₂

With oxalyl dichloride; hydrogen; toluene-4-sulfonic acid; dimethyl sulfoxide; triethylamine; N-ethyl-N,N-diisopropylamine; palladium on activated charcoal; In dichloromethane;
DOI:10.3987/R-1987-11-2805