1-[2-Chloro-5-(3,4-dimethoxy-phenyl)-oxazolidin-3-yl]-2-(3,4-dimethoxy-phenyl)-ethanone

Base Information

Chemical Name:1-[2-Chloro-5-(3,4-dimethoxy-phenyl)-oxazolidin-3-yl]-2-(3,4-dimethoxy-phenyl)-ethanone
CAS No.:78004-22-5
Molecular Formula:C₂₁H₂₄ClNO₆
Molecular Weight:421.878
Hs Code.:

Synonyms:1-[2-Chloro-5-(3,4-dimethoxy-phenyl)-oxazolidin-3-yl]-2-(3,4-dimethoxy-phenyl)-ethanone

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Chemical Property of 1-[2-Chloro-5-(3,4-dimethoxy-phenyl)-oxazolidin-3-yl]-2-(3,4-dimethoxy-phenyl)-ethanone

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Technology Process of 1-[2-Chloro-5-(3,4-dimethoxy-phenyl)-oxazolidin-3-yl]-2-(3,4-dimethoxy-phenyl)-ethanone

There total 2 articles about 1-[2-Chloro-5-(3,4-dimethoxy-phenyl)-oxazolidin-3-yl]-2-(3,4-dimethoxy-phenyl)-ethanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 120-14-9
3,4-dimethoxy-benzaldehyde

: 78004-22-5
1-[2-Chloro-5-(3,4-dimethoxy-phenyl)-oxazolidin-3-yl]-2-(3,4-dimethoxy-phenyl)-ethanone

Guidance literature:: Multi-step reaction with 2 steps

1: n-BuLi / 1.) THF, -78 deg C, 60 min; 2.) -60 deg C, 30 min

2: CH₂Cl₂ / 0.5 h

With n-butyllithium; In dichloromethane;
DOI:10.1021/jo00331a038

Reference yield:

: 10313-60-7
3,4-dimethoxyphenylacetyl chloride

: 78004-17-8
5-(3,4-Dimethoxyphenyl)-2-oxazoline

: 78004-22-5
1-[2-Chloro-5-(3,4-dimethoxy-phenyl)-oxazolidin-3-yl]-2-(3,4-dimethoxy-phenyl)-ethanone

Guidance literature:: In dichloromethane; for 0.5h;
DOI:10.1021/jo00331a038

Reference yield:

: 78004-22-5
1-[2-Chloro-5-(3,4-dimethoxy-phenyl)-oxazolidin-3-yl]-2-(3,4-dimethoxy-phenyl)-ethanone

: 58-74-2
Papaverine

Guidance literature:: Multi-step reaction with 2 steps

1: Et₃N, H₂₀ / CH₂Cl₂; tetrahydrofuran / 0.5 h

2: POCl₃ / acetonitrile / 1 h / Heating

With water; triethylamine; trichlorophosphate; In tetrahydrofuran; dichloromethane; acetonitrile;
DOI:10.1021/jo00331a038