Technology Process of C17H19Cl2N5O4
There total 5 articles about C17H19Cl2N5O4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
hydrogen;
10% palladium hydroxide on charcoal;
In
methanol;
at 20 ℃;
for 2h;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: trimethylsilylazide / 12 h / Reflux
2.1: triethylamine / tetrahydrofuran / 0.25 h / 20 °C / Inert atmosphere
2.2: 1 h / Reflux
3.1: hydrogen / 10% palladium hydroxide on charcoal / methanol / 2 h / 20 °C
With
trimethylsilylazide; hydrogen; triethylamine;
10% palladium hydroxide on charcoal;
In
tetrahydrofuran; methanol;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: potassium carbonate / N,N-dimethyl-formamide / 4 h / 20 °C / Inert atmosphere
2.1: sodium tris(acetoxy)borohydride / 1,2-dichloro-ethane; tetrahydrofuran / 1 h / 20 °C / Inert atmosphere
3.1: triethylamine / tetrahydrofuran / 0.25 h / 20 °C / Inert atmosphere
3.2: 1 h / Reflux
4.1: hydrogen / 10% palladium hydroxide on charcoal / methanol / 2 h / 20 °C
With
hydrogen; sodium tris(acetoxy)borohydride; potassium carbonate; triethylamine;
10% palladium hydroxide on charcoal;
In
tetrahydrofuran; methanol; 1,2-dichloro-ethane; N,N-dimethyl-formamide;