(2S,3R)-2,3-epoxy-8-methylnonyl (2R)-3,3,3-trifluoro-2-methoxy-2-phenylpropionate

Base Information

Chemical Name:(2S,3R)-2,3-epoxy-8-methylnonyl (2R)-3,3,3-trifluoro-2-methoxy-2-phenylpropionate
CAS No.:107996-54-3
Molecular Formula:C₂₀H₂₇F₃O₄
Molecular Weight:388.427
Hs Code.:

Synonyms:(2S,3R)-2,3-epoxy-8-methylnonyl (2R)-3,3,3-trifluoro-2-methoxy-2-phenylpropionate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2S,3R)-2,3-epoxy-8-methylnonyl (2R)-3,3,3-trifluoro-2-methoxy-2-phenylpropionate

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Technology Process of (2S,3R)-2,3-epoxy-8-methylnonyl (2R)-3,3,3-trifluoro-2-methoxy-2-phenylpropionate

There total 3 articles about (2S,3R)-2,3-epoxy-8-methylnonyl (2R)-3,3,3-trifluoro-2-methoxy-2-phenylpropionate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 20445-31-2
R-(+)-α-trifluoromethyl-α-methoxy-phenylacetic acid

: 81309-88-8
(2S,3R)-8-methyl-2,3-epoxynonan-1-ol

: 107996-54-3
(2S,3R)-2,3-epoxy-8-methylnonyl (2R)-3,3,3-trifluoro-2-methoxy-2-phenylpropionate

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; for 2.5h; Ambient temperature;

Reference yield:

: 107996-53-2
(2S,3R)-1-(3',5'-dinitrobenzoyloxy)-2,3-epoxy-8-methylnonane

: 107996-54-3
(2S,3R)-2,3-epoxy-8-methylnonyl (2R)-3,3,3-trifluoro-2-methoxy-2-phenylpropionate

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / potassium carbonate / methanol; tetrahydrofuran

2: 94 percent / N,N'-dicyclohexylcarbodiimide, 4-(dimethylamino)pyridine / CH₂Cl₂ / 2.5 h / Ambient temperature

With dmap; potassium carbonate; dicyclohexyl-carbodiimide; In tetrahydrofuran; methanol; dichloromethane;

Reference yield:

: 115937-04-7
2,3-epoxy-8-methyl-1-nonanol

: 107996-54-3
(2S,3R)-2,3-epoxy-8-methylnonyl (2R)-3,3,3-trifluoro-2-methoxy-2-phenylpropionate

Guidance literature:: Multi-step reaction with 3 steps

1: 52 percent / pyridine / diethyl ether / 4 h / 0 °C

2: 90 percent / potassium carbonate / methanol; tetrahydrofuran

3: 94 percent / N,N'-dicyclohexylcarbodiimide, 4-(dimethylamino)pyridine / CH₂Cl₂ / 2.5 h / Ambient temperature

With pyridine; dmap; potassium carbonate; dicyclohexyl-carbodiimide; In tetrahydrofuran; methanol; diethyl ether; dichloromethane;