(S)-[tert-butyl 4-((((9H-fluoren-9-yl)methoxy)carbonyl)amino)-5-(((S)-1-(((S)-1-amino-4-methyl-1-oxopentan-2-yl)amino)-3-(4-((bis(allyloxy)phosphoryl)oxy)-3-(fluoromethyl)phenyl)-1-oxopropan-2-yl)amino)-5-oxopentanoate]

Base Information

Chemical Name:(S)-[tert-butyl 4-((((9H-fluoren-9-yl)methoxy)carbonyl)amino)-5-(((S)-1-(((S)-1-amino-4-methyl-1-oxopentan-2-yl)amino)-3-(4-((bis(allyloxy)phosphoryl)oxy)-3-(fluoromethyl)phenyl)-1-oxopropan-2-yl)amino)-5-oxopentanoate]
CAS No.:1258428-91-9
Molecular Formula:C₄₆H₅₈FN₄O₁₁P
Molecular Weight:892.959
Hs Code.:

(S)-[tert-butyl 4-((((9H-fluoren-9-yl)methoxy)carbonyl)amino)-5-(((S)-1-(((S)-1-amino-4-methyl-1-oxopentan-2-yl)amino)-3-(4-((bis(allyloxy)phosphoryl)oxy)-3-(fluoromethyl)phenyl)-1-oxopropan-2-yl)amino)-5-oxopentanoate]

Synonyms:(S)-[tert-butyl 4-((((9H-fluoren-9-yl)methoxy)carbonyl)amino)-5-(((S)-1-(((S)-1-amino-4-methyl-1-oxopentan-2-yl)amino)-3-(4-((bis(allyloxy)phosphoryl)oxy)-3-(fluoromethyl)phenyl)-1-oxopropan-2-yl)amino)-5-oxopentanoate]

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Chemical Property of (S)-[tert-butyl 4-((((9H-fluoren-9-yl)methoxy)carbonyl)amino)-5-(((S)-1-(((S)-1-amino-4-methyl-1-oxopentan-2-yl)amino)-3-(4-((bis(allyloxy)phosphoryl)oxy)-3-(fluoromethyl)phenyl)-1-oxopropan-2-yl)amino)-5-oxopentanoate]

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Technology Process of (S)-[tert-butyl 4-((((9H-fluoren-9-yl)methoxy)carbonyl)amino)-5-(((S)-1-(((S)-1-amino-4-methyl-1-oxopentan-2-yl)amino)-3-(4-((bis(allyloxy)phosphoryl)oxy)-3-(fluoromethyl)phenyl)-1-oxopropan-2-yl)amino)-5-oxopentanoate]

There total 1 articles about (S)-[tert-butyl 4-((((9H-fluoren-9-yl)methoxy)carbonyl)amino)-5-(((S)-1-(((S)-1-amino-4-methyl-1-oxopentan-2-yl)amino)-3-(4-((bis(allyloxy)phosphoryl)oxy)-3-(fluoromethyl)phenyl)-1-oxopropan-2-yl)amino)-5-oxopentanoate] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1258428-86-2
C₂HF₃O₂*C₂₂H₃₃FN₃O₆P

: 71989-18-9
Fmoc-Glu(OtBu)-OH

: 1258428-91-9
(S)-[tert-butyl 4-((((9H-fluoren-9-yl)methoxy)carbonyl)amino)-5-(((S)-1-(((S)-1-amino-4-methyl-1-oxopentan-2-yl)amino)-3-(4-((bis(allyloxy)phosphoryl)oxy)-3-(fluoromethyl)phenyl)-1-oxopropan-2-yl)amino)-5-oxopentanoate]

Guidance literature:: With benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine; dicyclohexyl-carbodiimide; In N,N-dimethyl-formamide; at 20 ℃; Cooling with ice;
DOI:10.1016/j.tet.2010.04.065

Reference yield: 60.0%

: 108-30-5
succinic acid anhydride

: 1258428-91-9
(S)-[tert-butyl 4-((((9H-fluoren-9-yl)methoxy)carbonyl)amino)-5-(((S)-1-(((S)-1-amino-4-methyl-1-oxopentan-2-yl)amino)-3-(4-((bis(allyloxy)phosphoryl)oxy)-3-(fluoromethyl)phenyl)-1-oxopropan-2-yl)amino)-5-oxopentanoate]

: 1258428-92-0
4-(((S)-1-(((S)-1-(((S)-1-amino-4-methyl-1-oxopentan-2-yl)amino)-3-(4-((bis(allyloxy)phosphoryl)oxy)-3-(fluoromethyl)phenyl)-1-oxopropan-2-yl)amino)-5-(tert-butoxy)-1,5-dioxopentan-2-yl)amino)-4-oxobutanoic acid

Guidance literature:: (S)-[tert-butyl 4-((((9H-fluoren-9-yl)methoxy)carbonyl)amino)-5-(((S)-1-(((S)-1-amino-4-methyl-1-oxopentan-2-yl)amino)-3-(4-((bis(allyloxy)phosphoryl)oxy)-3-(fluoromethyl)phenyl)-1-oxopropan-2-yl)amino)-5-oxopentanoate]; With diethylamine; In dichloromethane; at 20 ℃; for 0.5h;

succinic acid anhydride; In dichloromethane; at 20 ℃; for 18h;
DOI:10.1016/j.tet.2010.04.065