11-amino-[11N-12O]carbonyl-N¹¹-amino-2'O-benzoyl-11-deshydroxy-10-desmethyl-10-ethyl-6-0-methyl-3-oxo-descladinosyl-erythromycin A

Base Information

• Chemical Name: 11-amino-[11N-12O]carbonyl-N¹¹-amino-2'O-benzoyl-11-deshydroxy-10-desmethyl-10-ethyl-6-0-methyl-3-oxo-descladinosyl-erythromycin A
• CAS No.: 717889-35-5
• Molecular Formula: C₃₉H₅₉N₃O₁₁
• Molecular Weight: 745.911

Synonyms:11-amino-[11N-12O]carbonyl-N¹¹-amino-2'O-benzoyl-11-deshydroxy-10-desmethyl-10-ethyl-6-0-methyl-3-oxo-descladinosyl-erythromycin A

Chemical Property of 11-amino-[11N-12O]carbonyl-N¹¹-amino-2'O-benzoyl-11-deshydroxy-10-desmethyl-10-ethyl-6-0-methyl-3-oxo-descladinosyl-erythromycin A

Chemical Property:

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Technology Process of 11-amino-[11N-12O]carbonyl-N¹¹-amino-2'O-benzoyl-11-deshydroxy-10-desmethyl-10-ethyl-6-0-methyl-3-oxo-descladinosyl-erythromycin A

There total 1 articles about 11-amino-[11N-12O]carbonyl-N¹¹-amino-2'O-benzoyl-11-deshydroxy-10-desmethyl-10-ethyl-6-0-methyl-3-oxo-descladinosyl-erythromycin A which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

10,11-anhydro-2'O-benzoyl-10-desmethyl-10-ethyl-12-O-(imidazolocarbonyl)-6-O-methyl-3-oxo-descladinosyl-erythromycin A → 11-amino-[11N-12O]carbonyl-N11-amino-2'O-benzoyl-11-deshydroxy-10-desmethyl-10-ethyl-6-0-methyl-3-oxo-descladinosyl-erythromycin A (717889-35-5)

Guidance literature:

With hydrazine; In DMF (N,N-dimethyl-formamide); at 20 ℃; for 3h;

Reference yield:

11-amino-[11N-12O]carbonyl-N11-amino-2'O-benzoyl-11-deshydroxy-10-desmethyl-10-ethyl-6-0-methyl-3-oxo-descladinosyl-erythromycin A (717889-35-5) + sodium cyanoborohydride (25895-60-7) → 11-amino-[11N-12O]carbonyl-2'O-benzoyl-11-deshydroxy-10-desmethyl-10-ethyl-6-O-methyl-3-oxo-N11-[3-(4-quinolinyl)propylamino]-descladinosyl-erythromycin A (717889-36-6)

Guidance literature:

11-amino-[11N-12O]carbonyl-N¹¹-amino-2'O-benzoyl-11-deshydroxy-10-desmethyl-10-ethyl-6-0-methyl-3-oxo-descladinosyl-erythromycin A; 3-(4-quinolinyl)propionaldehyde; With acetic acid; In methanol; at 20 ℃; for 5h;

sodium cyanoborohydride; In methanol; at 20 ℃;

With sodium carbonate; In methanol; water;

Downstream raw materials:

11-amino-[11N-12O]carbonyl-2'O-benzoyl-11-deshydroxy-10-desmethyl-10-ethyl-6-O-methyl-3-oxo-N¹¹-[3-(4-quinolinyl)propylamino]-descladinosyl-erythromycin A

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