(2-((2,6-diisopropylphenyl)amino)-4-((2,6-diisopropylphenyl)imino)pent-2-ene)ZnCl

Base Information

Chemical Name:(2-((2,6-diisopropylphenyl)amino)-4-((2,6-diisopropylphenyl)imino)pent-2-ene)ZnCl
CAS No.:359641-96-6
Molecular Formula:C₂₉H₄₁ClN₂Zn
Molecular Weight:518.501
Hs Code.:

Synonyms:(2-((2,6-diisopropylphenyl)amino)-4-((2,6-diisopropylphenyl)imino)pent-2-ene)ZnCl

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Chemical Property of (2-((2,6-diisopropylphenyl)amino)-4-((2,6-diisopropylphenyl)imino)pent-2-ene)ZnCl

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Technology Process of (2-((2,6-diisopropylphenyl)amino)-4-((2,6-diisopropylphenyl)imino)pent-2-ene)ZnCl

There total 3 articles about (2-((2,6-diisopropylphenyl)amino)-4-((2,6-diisopropylphenyl)imino)pent-2-ene)ZnCl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: (2-((2,6-diisopropylphenyl)amino)-4-((2,6-diisopropylphenyl)imino)pent-2-ene)Li*OEt₂

: 7646-85-7,24359-56-6
zinc(II) chloride

: 359641-96-6
(2-((2,6-diisopropylphenyl)amino)-4-((2,6-diisopropylphenyl)imino)pent-2-ene)ZnCl

Guidance literature:: In diethyl ether; under N2 atm. to suspn. ZnCl2 in Et2O was added slowly soln. (dipp)NacNacLi*OEt2 in Et2O at -78°C, mixt. was allowed to warm to room temp. and stirred for 3 h; react. mixt. was filtered and concd.; elem. anal.;
DOI:10.1021/om010301x

Reference yield: 92.0%

: (2-((2,6-diisopropylphenyl)amino)-4-((2,6-diisopropylphenyl)imino)pent-2-ene)Li*OEt₂

: 7646-85-7,24359-56-6
zinc(II) chloride

: 359641-96-6
(2-((2,6-diisopropylphenyl)amino)-4-((2,6-diisopropylphenyl)imino)pent-2-ene)ZnCl

: 473402-50-5
CH(CH₃CNC₆H₃(CH(CH₃)2)2)2ZnCl₂Li(O(C₂H₅)2)2

Guidance literature:: In diethyl ether; byproducts: LiCl; under inert atm., 1 equiv. of Li-compd. in Et2O was added to Et2O soln. of ZnCl2 at -78 °C, mixt. was allowed to warm to room temp., stirred for 3 h; mixt. was filtered, soln. was concd. in vac., storage at -24 °C for 2 d, elem. anal.;
DOI:10.1002/1099-0682(200208)2002:8<2156::AID-EJIC2156>3.0.CO;2-P