C₁₉H₂₅NO₅

Base Information

Chemical Name:C₁₉H₂₅NO₅
CAS No.:80515-96-4
Molecular Formula:C₁₉H₂₅NO₅
Molecular Weight:347.411
Hs Code.:

C<sub>19</sub>H<sub>25</sub>NO<sub>5</sub>

Synonyms:C₁₉H₂₅NO₅

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Chemical Property of C₁₉H₂₅NO₅

Chemical Property:

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Technology Process of C₁₉H₂₅NO₅

There total 25 articles about C₁₉H₂₅NO₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 21104-34-7
N-methyl-3a-<3,4-(dimethoxy)phenyl>-2,3,3a,4,5,6,7,7a-octahydroindole-2,6-dione

: 107-21-1
ethylene glycol

: 80515-96-4
C₁₉H₂₅NO₅

Guidance literature:: With toluene-4-sulfonic acid; In benzene; at 120 ℃; for 5h; Inert atmosphere; Dean-Stark;
DOI:10.1055/s-0036-1591547

Reference yield:

: 20036-53-7
3-<3,4-(dimethoxy)phenyl>-2-cyclohexen-1-one

: 80515-96-4
C₁₉H₂₅NO₅

Guidance literature:: Multi-step reaction with 12 steps

1: 89 percent / NaBH₄ / ethanol / 12 h / -20 °C

2: 76 percent / pyridine / 18 h / Ambient temperature

3: 1.) lithium isopropylcyclohexylamide, HMPA, 2.) tert-butyldimethylchlorosilane / 1.) THF, -78 deg C, 5 min, 2.) reflux, 3 h

4: 1.) SOCl₂, 2.) NH₂OH*HCl, Na₂CO₃ / 1.) benzene, DMF, reflux, 2 h, 2.) diethyl ether

5: 82.5 percent / tetrapropylammonium periodate / CHCl₃; dimethylformamide

6: 100 percent / toluene / 0.33 h / Heating

7: 78 percent / Na₂CO₃, TiCl₃ / H₂O; methanol / 18 h / Ambient temperature

8: 90 percent / NaH / tetrahydrofuran / 12 h / Ambient temperature

9: 88 percent / DME-H₂O, N-bromosuccinimide / 5 h / -18 °C

10: 90 percent / α,α'-azobis(isobutyronitrile), tributyltin hydride / benzene / 2.5 h / Heating

11: 85 percent / pyridinium chlorochromate / CH₂Cl₂ / 1.5 h / 4 °C

12: p-toluenesulfonic acid monohydrate / benzene / 96 h / Heating

With pyridine; N,N,N,N,N,N-hexamethylphosphoric triamide; sodium tetrahydroborate; N-Bromosuccinimide; thionyl chloride; titanium(III) chloride; tetrapropylammonium periodate; DME-H₂O; azobisisobutyronitrile; hydroxylamine hydrochloride; tri-n-butyl-tin hydride; sodium hydride; sodium carbonate; lithium cyclohexylisopropylamide; toluene-4-sulfonic acid; tert-butyldimethylsilyl chloride; pyridinium chlorochromate; In tetrahydrofuran; methanol; ethanol; dichloromethane; chloroform; water; N,N-dimethyl-formamide; toluene; benzene;
DOI:10.1021/jo00346a028

Reference yield:

: 2859-78-1
4-Bromoveratrole

: 80515-96-4
C₁₉H₂₅NO₅

Guidance literature:: Multi-step reaction with 13 steps

2: 89 percent / NaBH₄ / ethanol / 12 h / -20 °C

3: 76 percent / pyridine / 18 h / Ambient temperature

4: 1.) lithium isopropylcyclohexylamide, HMPA, 2.) tert-butyldimethylchlorosilane / 1.) THF, -78 deg C, 5 min, 2.) reflux, 3 h

5: 1.) SOCl₂, 2.) NH₂OH*HCl, Na₂CO₃ / 1.) benzene, DMF, reflux, 2 h, 2.) diethyl ether

6: 82.5 percent / tetrapropylammonium periodate / CHCl₃; dimethylformamide

7: 100 percent / toluene / 0.33 h / Heating

8: 78 percent / Na₂CO₃, TiCl₃ / H₂O; methanol / 18 h / Ambient temperature

9: 90 percent / NaH / tetrahydrofuran / 12 h / Ambient temperature

10: 88 percent / DME-H₂O, N-bromosuccinimide / 5 h / -18 °C

11: 90 percent / α,α'-azobis(isobutyronitrile), tributyltin hydride / benzene / 2.5 h / Heating

12: 85 percent / pyridinium chlorochromate / CH₂Cl₂ / 1.5 h / 4 °C

13: p-toluenesulfonic acid monohydrate / benzene / 96 h / Heating

With pyridine; N,N,N,N,N,N-hexamethylphosphoric triamide; sodium tetrahydroborate; N-Bromosuccinimide; thionyl chloride; titanium(III) chloride; tetrapropylammonium periodate; DME-H₂O; azobisisobutyronitrile; hydroxylamine hydrochloride; tri-n-butyl-tin hydride; sodium hydride; sodium carbonate; lithium cyclohexylisopropylamide; toluene-4-sulfonic acid; tert-butyldimethylsilyl chloride; pyridinium chlorochromate; In tetrahydrofuran; methanol; ethanol; dichloromethane; chloroform; water; N,N-dimethyl-formamide; toluene; benzene;
DOI:10.1021/jo00346a028