N,N'-(2-nitrobenzenesulfonamide)-N,N'-[6-((methoxycarbonyl)pyridin-2-yl)methyl]-1,2-diaminoethane

Base Information

Chemical Name:N,N'-(2-nitrobenzenesulfonamide)-N,N'-[6-((methoxycarbonyl)pyridin-2-yl)methyl]-1,2-diaminoethane
CAS No.:1450624-92-6
Molecular Formula:C₃₀H₂₈N₆O₁₂S₂
Molecular Weight:728.717
Hs Code.:

Synonyms:N,N'-(2-nitrobenzenesulfonamide)-N,N'-[6-((methoxycarbonyl)pyridin-2-yl)methyl]-1,2-diaminoethane

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Chemical Property of N,N'-(2-nitrobenzenesulfonamide)-N,N'-[6-((methoxycarbonyl)pyridin-2-yl)methyl]-1,2-diaminoethane

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Technology Process of N,N'-(2-nitrobenzenesulfonamide)-N,N'-[6-((methoxycarbonyl)pyridin-2-yl)methyl]-1,2-diaminoethane

There total 2 articles about N,N'-(2-nitrobenzenesulfonamide)-N,N'-[6-((methoxycarbonyl)pyridin-2-yl)methyl]-1,2-diaminoethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 42462-22-6
N-[2-(2-nitrophenylsulfonyl)aminoethyl]-2-nitrophenylsulfonamide

: 146462-25-1
methyl 6-(bromomethyl)picolinate

: 1450624-92-6
N,N'-(2-nitrobenzenesulfonamide)-N,N'-[6-((methoxycarbonyl)pyridin-2-yl)methyl]-1,2-diaminoethane

Guidance literature:: With sodium carbonate; In N,N-dimethyl-formamide; at 50 ℃; for 24h; Molecular sieve;
DOI:10.1021/ja4049493

Reference yield:

: 1694-92-4
2-Nitrobenzenesulfonyl chloride

: 1450624-92-6
N,N'-(2-nitrobenzenesulfonamide)-N,N'-[6-((methoxycarbonyl)pyridin-2-yl)methyl]-1,2-diaminoethane

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydrogencarbonate / tetrahydrofuran / 24 h / 20 °C / Cooling with ice

2: sodium carbonate / N,N-dimethyl-formamide / 24 h / 50 °C / Molecular sieve

With sodium hydrogencarbonate; sodium carbonate; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1021/ja4049493