3,4-dichloro-N-hydroxybenzenecarboximidoyl chloride

Base Information

• Chemical Name: 3,4-dichloro-N-hydroxybenzenecarboximidoyl chloride
• CAS No.: 1056189-27-5
• Molecular Formula: C₇H₄Cl₃NO
• Molecular Weight: 224.474
• Hs Code.: 2928009090
• Mol file: 1056189-27-5.mol

Synonyms:3,4-dichloro-N-hydroxybenzenecarboximidoyl chloride

Chemical Property of 3,4-dichloro-N-hydroxybenzenecarboximidoyl chloride

Chemical Property:

Purity/Quality:

97% ^*data from raw suppliers

3,4-Dichloro-α-chlorobenzaldoxime ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3,4-dichloro-N-hydroxybenzenecarboximidoyl chloride

There total 2 articles about 3,4-dichloro-N-hydroxybenzenecarboximidoyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

E-3,4-dichloro-benzaldehyde-oxime (5331-92-0) → 3,4-dichloro-N-hydroxybenzenecarboximidoyl chloride (1056189-27-5)

Guidance literature:

With N-chloro-succinimide; In N-methyl-acetamide; water;

Reference yield:

3,4-dichlorobenzaldehyde oxime (5331-92-0) → 3,4-dichloro-N-hydroxybenzenecarboximidoyl chloride (1056189-27-5)

Guidance literature:

With N-chloro-succinimide; In N,N-dimethyl-formamide; Ambient temperature;

DOI:10.1021/jm9803121

Reference yield:

propargyl alcohol (107-19-7) + 3,4-dichloro-N-hydroxybenzenecarboximidoyl chloride (1056189-27-5) → 3-(3,4-dichlorophenyl)-5-hydroxymethylisoxazole (6208-35-1)

Guidance literature:

With triethylamine; In dichloromethane; at 0 - 20 ℃; Yield given;

DOI:10.1021/jm9803121

upstream raw materials:

3,4-dichlorobenzaldehyde oxime

E-3,4-dichloro-benzaldehyde-oxime

Downstream raw materials:

3-(3,4-dichlorophenyl)-5-hydroxymethylisoxazole

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