S-[5-(5-amino-3-trifluoromethyl-1H-1,2,4-triazol-1-yl)-4-fluoro-2-methylphenyl]-2,2,2-trifluoroethylthiol

Base Information

Chemical Name:S-[5-(5-amino-3-trifluoromethyl-1H-1,2,4-triazol-1-yl)-4-fluoro-2-methylphenyl]-2,2,2-trifluoroethylthiol
CAS No.:885026-46-0
Molecular Formula:C₁₂H₉F₇N₄S
Molecular Weight:374.285
Hs Code.:

Synonyms:S-[5-(5-amino-3-trifluoromethyl-1H-1,2,4-triazol-1-yl)-4-fluoro-2-methylphenyl]-2,2,2-trifluoroethylthiol

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Chemical Property of S-[5-(5-amino-3-trifluoromethyl-1H-1,2,4-triazol-1-yl)-4-fluoro-2-methylphenyl]-2,2,2-trifluoroethylthiol

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Technology Process of S-[5-(5-amino-3-trifluoromethyl-1H-1,2,4-triazol-1-yl)-4-fluoro-2-methylphenyl]-2,2,2-trifluoroethylthiol

There total 2 articles about S-[5-(5-amino-3-trifluoromethyl-1H-1,2,4-triazol-1-yl)-4-fluoro-2-methylphenyl]-2,2,2-trifluoroethylthiol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 353-83-3
1,1,1-trifluoro-2-iodoethane

: 1158982-20-7
5-(5-amino-3-trifluoromethyl-1H-1,2,4-triazol-1-yl)-4-fluoro-2-methylthiophenol

: 885026-46-0
S-[5-(5-amino-3-trifluoromethyl-1H-1,2,4-triazol-1-yl)-4-fluoro-2-methylphenyl]-2,2,2-trifluoroethylthiol

Guidance literature:: With rongalite; potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 16h;

Reference yield:

: 885028-73-9
N-{2-fluoro-4-methyl-5-(2,2,2-trifluoroethylthio)phenyl}trifluoroacetohydrazonoyl bromide

: 4338-95-8
S-methylthiouronium iodide

: 885026-46-0
S-[5-(5-amino-3-trifluoromethyl-1H-1,2,4-triazol-1-yl)-4-fluoro-2-methylphenyl]-2,2,2-trifluoroethylthiol

Guidance literature:: N-{2-fluoro-4-methyl-5-(2,2,2-trifluoroethylthio)phenyl}trifluoroacetohydrazonoyl bromide; S-methylthiouronium iodide; With triethylamine; In tetrahydrofuran; for 8h; Heating / reflux;

In xylene; for 2h; Heating / reflux;