2-({bis[2-(trifluoromethyl)phenyl]phosphoryl}methyl)-6-[(1,3-dioxoisoindolin-2-yl)methyl]pyridine 1-oxide

Base Information

Chemical Name:2-({bis[2-(trifluoromethyl)phenyl]phosphoryl}methyl)-6-[(1,3-dioxoisoindolin-2-yl)methyl]pyridine 1-oxide
CAS No.:1620658-22-1
Molecular Formula:C₂₉H₁₉F₆N₂O₄P
Molecular Weight:604.445
Hs Code.:

Synonyms:2-({bis[2-(trifluoromethyl)phenyl]phosphoryl}methyl)-6-[(1,3-dioxoisoindolin-2-yl)methyl]pyridine 1-oxide

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Chemical Property of 2-({bis[2-(trifluoromethyl)phenyl]phosphoryl}methyl)-6-[(1,3-dioxoisoindolin-2-yl)methyl]pyridine 1-oxide

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Technology Process of 2-({bis[2-(trifluoromethyl)phenyl]phosphoryl}methyl)-6-[(1,3-dioxoisoindolin-2-yl)methyl]pyridine 1-oxide

There total 6 articles about 2-({bis[2-(trifluoromethyl)phenyl]phosphoryl}methyl)-6-[(1,3-dioxoisoindolin-2-yl)methyl]pyridine 1-oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 1620658-20-9
2-{[6-({bis[2-(trifluoromethyl)phenyl]phosphoryl}methyl)pyridin-2-yl]methyl}isoindoline-1,3-dione

: 1620658-22-1
2-({bis[2-(trifluoromethyl)phenyl]phosphoryl}methyl)-6-[(1,3-dioxoisoindolin-2-yl)methyl]pyridine 1-oxide

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 23 ℃; for 18h; Inert atmosphere; Schlenk technique;
DOI:10.1002/ejoc.201400120

Reference yield:

: 628308-52-1
2-{[6-(chloromethyl)pyridin-2-yl]methyl}isoindoline-1,3-dione

: 1620658-22-1
2-({bis[2-(trifluoromethyl)phenyl]phosphoryl}methyl)-6-[(1,3-dioxoisoindolin-2-yl)methyl]pyridine 1-oxide

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran / 12 h / 23 - 120 °C / Inert atmosphere; Schlenk technique

2: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 18 h / 23 °C / Inert atmosphere; Schlenk technique

With 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; dichloromethane;
DOI:10.1002/ejoc.201400120

Reference yield:

: 3099-28-3
2,6-bis(chloromethyl)pyridine

: 1620658-22-1
2-({bis[2-(trifluoromethyl)phenyl]phosphoryl}methyl)-6-[(1,3-dioxoisoindolin-2-yl)methyl]pyridine 1-oxide

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydrogencarbonate / N,N-dimethyl-formamide / 3 h / 23 °C / Inert atmosphere; Schlenk technique

2: tetrahydrofuran / 12 h / 23 - 120 °C / Inert atmosphere; Schlenk technique

3: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 18 h / 23 °C / Inert atmosphere; Schlenk technique

With sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/ejoc.201400120