C₃₃H₃₉F₃N₂O₇

Base Information

Chemical Name:C₃₃H₃₉F₃N₂O₇
CAS No.:174258-37-8
Molecular Formula:C₃₃H₃₉F₃N₂O₇
Molecular Weight:632.677
Hs Code.:

C<sub>33</sub>H<sub>39</sub>F<sub>3</sub>N<sub>2</sub>O<sub>7</sub>

Synonyms:C₃₃H₃₉F₃N₂O₇

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₃H₃₉F₃N₂O₇

Chemical Property:

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Technology Process of C₃₃H₃₉F₃N₂O₇

There total 9 articles about C₃₃H₃₉F₃N₂O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 85006-25-3
N,N-di(tert-butoxycarbonyl)hydroxylamine

: 174258-47-0
(Z)-3-{3-[5-methyl-2-(4-trifluoromethyl-phenyl)-oxazol-4-ylmethoxy]-phenyl}-pent-2-en-1-ol

: 174258-37-8
C₃₃H₃₉F₃N₂O₇

Guidance literature:: With triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; at 0 ℃; for 1h;
DOI:10.1021/jm990476x

Reference yield:

: 455-19-6
4-Trifluoromethylbenzaldehyde

: 174258-37-8
C₃₃H₃₉F₃N₂O₇

Guidance literature:: Multi-step reaction with 8 steps

1.1: 65 percent / HCl gas / ethyl acetate / 3 h / 5 °C

2.1: 30 percent / POCl₃ / CHCl₃ / 2.5 h / Heating

3.1: 65 percent / K₂CO₃ / dimethylformamide / 3 h / 80 °C

4.1: tetrahydrofuran / 0.5 h / 0 °C

5.1: Jones reagent / acetone / 0.5 h / 5 °C

6.1: NaH / toluene / 1 h

6.2: toluene; tetrahydrofuran / 48 h

7.1: DIBAL / diethyl ether / 0.5 h / -78 °C

8.1: diethyl azodicarboxylate; Ph₃P / tetrahydrofuran / 1 h / 0 °C

With hydrogenchloride; jones reagent; sodium hydride; diisobutylaluminium hydride; potassium carbonate; triphenylphosphine; diethylazodicarboxylate; trichlorophosphate; In tetrahydrofuran; diethyl ether; chloroform; ethyl acetate; N,N-dimethyl-formamide; acetone; toluene; 1.1: Condensation / 2.1: Chlorination / 3.1: Alkylation / 4.1: Grignard reaction / 5.1: Oxidation / 6.1: Metallation / 6.2: Condensation / 7.1: Reduction / 8.1: Condensation;
DOI:10.1021/jm990476x

Reference yield:

: 100-83-4
meta-hydroxybenzaldehyde

: 174258-37-8
C₃₃H₃₉F₃N₂O₇

Guidance literature:: Multi-step reaction with 6 steps

1.1: 65 percent / K₂CO₃ / dimethylformamide / 3 h / 80 °C

2.1: tetrahydrofuran / 0.5 h / 0 °C

3.1: Jones reagent / acetone / 0.5 h / 5 °C

4.1: NaH / toluene / 1 h

4.2: toluene; tetrahydrofuran / 48 h

5.1: DIBAL / diethyl ether / 0.5 h / -78 °C

6.1: diethyl azodicarboxylate; Ph₃P / tetrahydrofuran / 1 h / 0 °C

With jones reagent; sodium hydride; diisobutylaluminium hydride; potassium carbonate; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; diethyl ether; N,N-dimethyl-formamide; acetone; toluene; 1.1: Alkylation / 2.1: Grignard reaction / 3.1: Oxidation / 4.1: Metallation / 4.2: Condensation / 5.1: Reduction / 6.1: Condensation;
DOI:10.1021/jm990476x