(S)-methyl 2-(⁽²⁾-2(((benzyloxy)carbonyl)amino)-4-(methylthio)butanamido)propanoate

Base Information

• Chemical Name: (S)-methyl 2-(⁽²⁾-2(((benzyloxy)carbonyl)amino)-4-(methylthio)butanamido)propanoate
• CAS No.: 17664-84-5
• Molecular Formula: C₁₇H₂₄N₂O₅S
• Molecular Weight: 368.454

Synonyms:(S)-methyl 2-(⁽²⁾-2(((benzyloxy)carbonyl)amino)-4-(methylthio)butanamido)propanoate

Chemical Property of (S)-methyl 2-(⁽²⁾-2(((benzyloxy)carbonyl)amino)-4-(methylthio)butanamido)propanoate

Chemical Property:

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Technology Process of (S)-methyl 2-(⁽²⁾-2(((benzyloxy)carbonyl)amino)-4-(methylthio)butanamido)propanoate

There total 2 articles about (S)-methyl 2-(⁽²⁾-2(((benzyloxy)carbonyl)amino)-4-(methylthio)butanamido)propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

L-Alanine methyl ester (10065-72-2) + Cbz-Met-OH (1152-62-1) → (S)-methyl 2-((2)-2(((benzyloxy)carbonyl)amino)-4-(methylthio)butanamido)propanoate (17664-84-5)

Guidance literature:

Cbz-Met-OH; With (E)-ethyl 2-cyano-2-(2-nitrophenylsulfonyloxyimino)acetate; N-ethyl-N,N-diisopropylamine; In dichloromethane; at 25 ℃;

L-Alanine methyl ester; In dichloromethane; at 25 ℃;

DOI:10.1021/jo500292m

Reference yield: 84.0%

Cbz-Met-OH (1152-62-1) + (S)-methyl 2-(1H-imidazole-1-carboxamido)propanoate (93644-94-1) → (S)-methyl 2-((2)-2(((benzyloxy)carbonyl)amino)-4-(methylthio)butanamido)propanoate (17664-84-5)

Guidance literature:

With benzotriazol-1-ol; copper(ll) bromide; In dichloromethane; at 22 ℃; for 20h; Inert atmosphere; Schlenk technique;

DOI:10.1002/anie.201402147

upstream raw materials:

L-Alanine methyl ester

Cbz-Met-OH

(S)-methyl 2-(1H-imidazole-1-carboxamido)propanoate

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