methyl α-methylene-β-[(p-toluenesulfonyl)amino]-3-(4-methoxyphenyl)propionate

Base Information

Chemical Name:methyl α-methylene-β-[(p-toluenesulfonyl)amino]-3-(4-methoxyphenyl)propionate
CAS No.:364364-52-3
Molecular Formula:C₁₉H₂₁NO₅S
Molecular Weight:375.445
Hs Code.:

Synonyms:methyl α-methylene-β-[(p-toluenesulfonyl)amino]-3-(4-methoxyphenyl)propionate

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Chemical Property of methyl α-methylene-β-[(p-toluenesulfonyl)amino]-3-(4-methoxyphenyl)propionate

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Technology Process of methyl α-methylene-β-[(p-toluenesulfonyl)amino]-3-(4-methoxyphenyl)propionate

There total 1 articles about methyl α-methylene-β-[(p-toluenesulfonyl)amino]-3-(4-methoxyphenyl)propionate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 14674-38-5,135822-88-7
(E)-N-(4-methoxybenzylidene)-4-methylbenzenesulfonamide

: 292638-85-8,9003-21-8,96-33-3
acrylic acid methyl ester

: 364364-52-3
methyl α-methylene-β-[(p-toluenesulfonyl)amino]-3-(4-methoxyphenyl)propionate

Guidance literature:: With hydroxyl ionic liquid-supported quinuclidine; at 20 ℃; for 8h;
DOI:10.1016/j.tet.2005.12.045

Reference yield:

: 106-95-6
allyl bromide

: 364364-52-3
methyl α-methylene-β-[(p-toluenesulfonyl)amino]-3-(4-methoxyphenyl)propionate

: methyl-2-{[(N-allyl-4-methylphenyl)sulfonamido](4-methoxyphenyl)methyl}acrylate

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃;
DOI:10.1016/j.tetlet.2004.02.100

Reference yield:

: 364364-52-3
methyl α-methylene-β-[(p-toluenesulfonyl)amino]-3-(4-methoxyphenyl)propionate

: methyl 2-(4-methoxyphenyl)-1-tosyl-2,5-dihydro-1H-pyrrole-3-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: K₂CO₃ / dimethylformamide / 20 °C

2: 78 percent / (Cy)3PRuCl₂(=CHPh)(1,3-(Mes)2imidazolidin-2-yl) / CH₂Cl₂ / 0.02 h / 100 °C / microwave irradiation

With potassium carbonate; tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.tetlet.2004.02.100