Fe(CO)3(CNC₆H₁₁)2

Base Information

Chemical Name:Fe(CO)3(CNC₆H₁₁)2
CAS No.:25792-38-5
Molecular Formula:C₁₇H₂₂FeN₂O₃
Molecular Weight:358.22
Hs Code.:

Synonyms:Fe(CO)3(CNC₆H₁₁)2

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Chemical Property of Fe(CO)3(CNC₆H₁₁)2

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Technology Process of Fe(CO)3(CNC₆H₁₁)2

There total 3 articles about Fe(CO)3(CNC₆H₁₁)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 931-53-3
Cyclohexyl isocyanide

: 19706-02-6,34871-29-9
[Fe(CO)4(CNC₆H₁₁)]

: 25792-38-5
Fe(CO)3(CNC₆H₁₁)2

Guidance literature:: With trimethylamine N-oxide; In benzene; byproducts: CO; soln. of Fe complex, isonitrile and Me3NO refluxed for 20 min, under Ar; cooled, chromd. (silica, benzene), evapd.;

Reference yield: 10.0%

: 538-75-0
dicyclohexyl-carbodiimide

: 100447-70-9
triiron dodecacarbonyl

: 25792-38-5
Fe(CO)3(CNC₆H₁₁)2

: 19706-02-6,34871-29-9
Fe(CO)4(CNC₆H₁₁)

: 82044-62-0
[Fe2(CO)6(μ,μ'-(C6H11N)2CFe(CO)4)]

: 34871-26-6
[Fe2(CO)6(μ,μ'-(C6H11N)2CNC6H11)]

Guidance literature:: In n-heptane; under N2, soln. of Fe complex and dicyclohexylcarbodiimide in heptane heated to reflux until green color disappeared; filtered, solvent removed under reduced pressure, residue redissolved in hexane, chromd., recrystd. from hexane, elem. anal.;

Reference yield:

: 931-53-3
Cyclohexyl isocyanide

: 19706-02-6,34871-29-9
Fe(CO)4(CNC₆H₁₁)

: 25792-38-5
Fe(CO)3(CNC₆H₁₁)2

Guidance literature:: palladium(II) oxide; In benzene; byproducts: CO; The mixt. of complex and catalyst in benzene was heated to reflux and then t-BuNC was added; 2 min; influence of differ catalysts on this reaction;; not sepd., detected by IR-spectra;;
DOI:10.1016/0022-328X(87)87126-7