3,5-dinitro-2-<6-(1,3,4,5-tetraacetoxycyclohexane-1-carbonylamino)hexylamino>benzoic acid

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Chemical Name:3,5-dinitro-2-<6-(1,3,4,5-tetraacetoxycyclohexane-1-carbonylamino)hexylamino>benzoic acid
CAS No.:87363-52-8
Molecular Formula:C₂₈H₃₆N₄O₁₅
Molecular Weight:668.612
Hs Code.:

Synonyms:3,5-dinitro-2-<6-(1,3,4,5-tetraacetoxycyclohexane-1-carbonylamino)hexylamino>benzoic acid

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Chemical Property of 3,5-dinitro-2-<6-(1,3,4,5-tetraacetoxycyclohexane-1-carbonylamino)hexylamino>benzoic acid

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Technology Process of 3,5-dinitro-2-<6-(1,3,4,5-tetraacetoxycyclohexane-1-carbonylamino)hexylamino>benzoic acid

There total 3 articles about 3,5-dinitro-2-<6-(1,3,4,5-tetraacetoxycyclohexane-1-carbonylamino)hexylamino>benzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 87396-23-4
1,2,3-benzotriazol-1-yl D(-)-1,3,4,5-tetraacetoxycyclohexane-1-carboxylate

: N¹-(2-carboxy-4,6-dinitrophenyl)-1,6-hexanediamine hydrochloride

: 87363-52-8
3,5-dinitro-2-<6-(1,3,4,5-tetraacetoxycyclohexane-1-carbonylamino)hexylamino>benzoic acid

Guidance literature:: With triethylamine; In dichloromethane; N,N-dimethyl-formamide; for 5h;
DOI:10.1002/hlca.19830660413

Reference yield:

: 77-95-2
D-(-)-quinic acid

: 87363-52-8
3,5-dinitro-2-<6-(1,3,4,5-tetraacetoxycyclohexane-1-carbonylamino)hexylamino>benzoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 98 percent / 4-(dimethylamino)pyridine / pyridine / 24 h / Ambient temperature

2: 93 percent / N,N'-dicyclohexylcarbodiimide / CH₂Cl₂; tetrahydrofuran / 1.) 5 deg C, 1 h; 2.) r.t., 2 h

3: 76 percent / triethylamine / CH₂Cl₂; dimethylformamide / 5 h

With dmap; triethylamine; dicyclohexyl-carbodiimide; In tetrahydrofuran; pyridine; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/hlca.19830660413

Reference yield:

: 32469-24-2
(1R,3R,4R,5R)-(-)-quinic acid tetraacetate

: 87363-52-8
3,5-dinitro-2-<6-(1,3,4,5-tetraacetoxycyclohexane-1-carbonylamino)hexylamino>benzoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / N,N'-dicyclohexylcarbodiimide / CH₂Cl₂; tetrahydrofuran / 1.) 5 deg C, 1 h; 2.) r.t., 2 h

2: 76 percent / triethylamine / CH₂Cl₂; dimethylformamide / 5 h

With triethylamine; dicyclohexyl-carbodiimide; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/hlca.19830660413