4,4,5,5-tetramethyl-2-(3-methyl-1-phenyl-3,4-nonadien-5-yl)-[1,3,2]dioxaborolane

Base Information

Chemical Name:4,4,5,5-tetramethyl-2-(3-methyl-1-phenyl-3,4-nonadien-5-yl)-[1,3,2]dioxaborolane
CAS No.:1082069-23-5
Molecular Formula:C₂₂H₃₃BO₂
Molecular Weight:340.314
Hs Code.:

Synonyms:4,4,5,5-tetramethyl-2-(3-methyl-1-phenyl-3,4-nonadien-5-yl)-[1,3,2]dioxaborolane

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Chemical Property of 4,4,5,5-tetramethyl-2-(3-methyl-1-phenyl-3,4-nonadien-5-yl)-[1,3,2]dioxaborolane

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Technology Process of 4,4,5,5-tetramethyl-2-(3-methyl-1-phenyl-3,4-nonadien-5-yl)-[1,3,2]dioxaborolane

There total 3 articles about 4,4,5,5-tetramethyl-2-(3-methyl-1-phenyl-3,4-nonadien-5-yl)-[1,3,2]dioxaborolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 110211-29-5
PhCH₂CH₂CMe(OOCMe)CCBu

: 73183-34-3
bis(pinacol)diborane

: 1082069-23-5
4,4,5,5-tetramethyl-2-(3-methyl-1-phenyl-3,4-nonadien-5-yl)-[1,3,2]dioxaborolane

Guidance literature:: With copper (I) tert-butoxide; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; In tetrahydrofuran; at 50 ℃; for 24h; Inert atmosphere;
DOI:10.1021/ja806602h

Reference yield: 53.0%

: PhCH₂CH₂CMe(OMe)CCBu

: 73183-34-3
bis(pinacol)diborane

: 1082069-23-5
4,4,5,5-tetramethyl-2-(3-methyl-1-phenyl-3,4-nonadien-5-yl)-[1,3,2]dioxaborolane

Guidance literature:: With copper (I) tert-butoxide; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; In tetrahydrofuran; at 50 ℃; for 48h; Inert atmosphere;
DOI:10.1021/ja806602h

Reference yield: 1.0%

: 1082069-22-4
methyl 3-methyl-1-phenyl-4-nonyn-3-yl carbonate

: 73183-34-3
bis(pinacol)diborane

: 1082069-23-5
4,4,5,5-tetramethyl-2-(3-methyl-1-phenyl-3,4-nonadien-5-yl)-[1,3,2]dioxaborolane

Guidance literature:: copper (I) tert-butoxide; In tetrahydrofuran; reaction of boron compd. with 2 equiv. of acetylene deriv. in THF in presence of copper compd. at 50°C for 1 h;
DOI:10.1021/ja806602h