5-(5-(4-(4-methoxybenzylthio)phenyl)-1,2,4-oxadiazol-3-yl)-1-(3-(2-methoxyethoxy)benzyl)pyridin-2(1H)-one

Base Information

Chemical Name:5-(5-(4-(4-methoxybenzylthio)phenyl)-1,2,4-oxadiazol-3-yl)-1-(3-(2-methoxyethoxy)benzyl)pyridin-2(1H)-one
CAS No.:1571033-60-7
Molecular Formula:C₃₁H₂₉N₃O₅S
Molecular Weight:555.654
Hs Code.:

Synonyms:5-(5-(4-(4-methoxybenzylthio)phenyl)-1,2,4-oxadiazol-3-yl)-1-(3-(2-methoxyethoxy)benzyl)pyridin-2(1H)-one

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Chemical Property of 5-(5-(4-(4-methoxybenzylthio)phenyl)-1,2,4-oxadiazol-3-yl)-1-(3-(2-methoxyethoxy)benzyl)pyridin-2(1H)-one

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Technology Process of 5-(5-(4-(4-methoxybenzylthio)phenyl)-1,2,4-oxadiazol-3-yl)-1-(3-(2-methoxyethoxy)benzyl)pyridin-2(1H)-one

There total 1 articles about 5-(5-(4-(4-methoxybenzylthio)phenyl)-1,2,4-oxadiazol-3-yl)-1-(3-(2-methoxyethoxy)benzyl)pyridin-2(1H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.7%

: 252973-46-9
4-[(4-methoxyphenyl)thio]benzoic acid

: 1571032-97-7,1571033-57-2
(Z)-N'-hydroxy-1-(3-(2-methoxyethoxy)benzyl)-6-oxo-1,6-dihydropyridine-3-carboximidamide

: 1571033-60-7
5-(5-(4-(4-methoxybenzylthio)phenyl)-1,2,4-oxadiazol-3-yl)-1-(3-(2-methoxyethoxy)benzyl)pyridin-2(1H)-one

Guidance literature:: With potassium carbonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In N,N-dimethyl-formamide; at 110 ℃; for 16h;

Reference yield: 81.0%

: 1571033-60-7
5-(5-(4-(4-methoxybenzylthio)phenyl)-1,2,4-oxadiazol-3-yl)-1-(3-(2-methoxyethoxy)benzyl)pyridin-2(1H)-one

: 1571033-66-3
5-(5-(4-mercaptophenyl)-1,2,4-oxadiazol-3-yl)-1-(3-(2-methoxyethoxy)benzyl)pyridin-2(1H)-one

Guidance literature:: With Triethoxysilane; trifluoroacetic acid; at 80 ℃; for 16h;

Reference yield:

: 1571033-60-7
5-(5-(4-(4-methoxybenzylthio)phenyl)-1,2,4-oxadiazol-3-yl)-1-(3-(2-methoxyethoxy)benzyl)pyridin-2(1H)-one

: 1571024-53-7
2-(4-(3-(1-(3-(2-methoxyethoxy)benzyl)-6-oxo-1,6-dihydropyridin-3-yl)-1,2,4-oxadiazol-5-yl)phenylsulfonyl)acetonitrile

Guidance literature:: Multi-step reaction with 3 steps

1: Triethoxysilane; trifluoroacetic acid / 16 h / 80 °C

2: potassium carbonate / N,N-dimethyl-formamide / 16 h / 55 °C

3: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 2 h / 20 °C

With Triethoxysilane; potassium carbonate; 3-chloro-benzenecarboperoxoic acid; trifluoroacetic acid; In dichloromethane; N,N-dimethyl-formamide;