(S)-2-(N,N-dibenzylamino)-5-pentane-1,5-diyl bis(2,2,4,4-tetrametyl-1,3-oxazolidine-3-carboxylate)

Base Information

Chemical Name:(S)-2-(N,N-dibenzylamino)-5-pentane-1,5-diyl bis(2,2,4,4-tetrametyl-1,3-oxazolidine-3-carboxylate)
CAS No.:167905-38-6
Molecular Formula:C₃₅H₅₁N₃O₆
Molecular Weight:609.806
Hs Code.:

Synonyms:(S)-2-(N,N-dibenzylamino)-5-pentane-1,5-diyl bis(2,2,4,4-tetrametyl-1,3-oxazolidine-3-carboxylate)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-2-(N,N-dibenzylamino)-5-pentane-1,5-diyl bis(2,2,4,4-tetrametyl-1,3-oxazolidine-3-carboxylate)

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Technology Process of (S)-2-(N,N-dibenzylamino)-5-pentane-1,5-diyl bis(2,2,4,4-tetrametyl-1,3-oxazolidine-3-carboxylate)

There total 2 articles about (S)-2-(N,N-dibenzylamino)-5-pentane-1,5-diyl bis(2,2,4,4-tetrametyl-1,3-oxazolidine-3-carboxylate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 146176-60-5
2,2,4,4-tetramethyl-1,3-oxazolidine-3-carbonyl chloride

: 142784-66-5
(S)-2-(N,N-dibenzylamino)-1,5-pentanediol

: 167905-38-6
(S)-2-(N,N-dibenzylamino)-5-pentane-1,5-diyl bis(2,2,4,4-tetrametyl-1,3-oxazolidine-3-carboxylate)

Guidance literature:: With sodium hydride;

Reference yield:

: 167905-35-3
(S)-2-dibenzylaminopentanedioic acid dibenzyl ester

: 167905-38-6
(S)-2-(N,N-dibenzylamino)-5-pentane-1,5-diyl bis(2,2,4,4-tetrametyl-1,3-oxazolidine-3-carboxylate)

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / LiAlH₄

2: 79 percent / NaH

With lithium aluminium tetrahydride; sodium hydride;

Reference yield:

: 167905-38-6
(S)-2-(N,N-dibenzylamino)-5-pentane-1,5-diyl bis(2,2,4,4-tetrametyl-1,3-oxazolidine-3-carboxylate)

: 74-88-4
methyl iodide

: (2S,5S)-2-(N,N-dibenzylamino)-5-methylpentane-1,5-diyl bis(2,2,4,4-tetramethyl-1,3-oxazolidyne-3-carboxylate)

: (2S,5R)-2-(N,N-dibenzylamino)-5-methylpentane-1,5-diyl bis(2,2,4,4-tetramethyl-1,3-oxazolidyne-3-carboxylate)

Guidance literature:: (S)-2-(N,N-dibenzylamino)-5-pentane-1,5-diyl bis(2,2,4,4-tetrametyl-1,3-oxazolidine-3-carboxylate); With sec.-butyllithium; (-)-sparteine; In diethyl ether; hexane; cyclohexane; at -78 ℃; for 7h;

methyl iodide; In diethyl ether; hexane; cyclohexane; at -78 - 20 ℃; for 14h; Further stages. Title compound not separated from byproducts.;
DOI:10.1055/s-2007-983724