5-cyclohexenylnicotinaldehyde

Base Information

Chemical Name:5-cyclohexenylnicotinaldehyde
CAS No.:1308869-87-5
Molecular Formula:C₁₂H₁₃NO
Molecular Weight:187.241
Hs Code.:

Synonyms:5-cyclohexenylnicotinaldehyde

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Chemical Property of 5-cyclohexenylnicotinaldehyde

Chemical Property:

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Technology Process of 5-cyclohexenylnicotinaldehyde

There total 1 articles about 5-cyclohexenylnicotinaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 113118-81-3
5-bromopyridine-3-carbaldehyde

: 89490-05-1,21190-87-4
cyclohex-1-enylboronic acid

: 1308869-87-5
5-cyclohexenylnicotinaldehyde

Guidance literature:: With potassium acetate; bis(di-tert-?butyl(4-?dimethylaminophenyl)?phosphine)?dichloropalladium(II); In ethanol; water; at 80 ℃; for 18h; Inert atmosphere;

Reference yield:

: 1308869-91-1
((6-bromo-2-chloroquinolin-3-yl)methyl)triphenylphosphonium chloride

: 1308869-87-5
5-cyclohexenylnicotinaldehyde

: 1308869-93-3
6-bromo-2-chloro-3-(2-(5-cyclohexenylpyridin-3-yl)vinyl)quinoline

Guidance literature:: With potassium carbonate; In dimethyl sulfoxide; at 70 ℃; for 1h;

Reference yield:

: 1308869-87-5
5-cyclohexenylnicotinaldehyde

: 1308869-08-0
3-(2-(5-cyclohexylpyridin-3-yl)ethyl)-6-o-tolylquinolin-2-amine

Guidance literature:: Multi-step reaction with 5 steps

1: potassium carbonate / dimethyl sulfoxide / 1 h / 70 °C

2: 1-methyl-pyrrolidin-2-one / 0.5 h / 200 °C / Microwave irradiation

3: trifluoroacetic acid / 1 h / 90 °C

4: potassium acetate / bis(di-tert-?butyl(4-?dimethylaminophenyl)?phosphine)?dichloropalladium(II) / ethanol; water / 2 h / 100 °C

5: hydrogen / palladium 10% on activated carbon / dichloromethane; ethanol / 12 h / Inert atmosphere

With hydrogen; potassium acetate; potassium carbonate; trifluoroacetic acid; bis(di-tert-?butyl(4-?dimethylaminophenyl)?phosphine)?dichloropalladium(II); palladium 10% on activated carbon; In 1-methyl-pyrrolidin-2-one; ethanol; dichloromethane; water; dimethyl sulfoxide;