N,N'-bis(3-tert-butyl-5-methoxy-2-hydroxyphenylmethyl)-N,N'-dimethylethylenediamine

Base Information

Chemical Name:N,N'-bis(3-tert-butyl-5-methoxy-2-hydroxyphenylmethyl)-N,N'-dimethylethylenediamine
CAS No.:1305347-30-1
Molecular Formula:C₂₈H₄₄N₂O₄
Molecular Weight:472.668
Hs Code.:

Synonyms:N,N'-bis(3-tert-butyl-5-methoxy-2-hydroxyphenylmethyl)-N,N'-dimethylethylenediamine

Suppliers and Price of N,N'-bis(3-tert-butyl-5-methoxy-2-hydroxyphenylmethyl)-N,N'-dimethylethylenediamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N,N'-bis(3-tert-butyl-5-methoxy-2-hydroxyphenylmethyl)-N,N'-dimethylethylenediamine

Chemical Property:

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Technology Process of N,N'-bis(3-tert-butyl-5-methoxy-2-hydroxyphenylmethyl)-N,N'-dimethylethylenediamine

There total 2 articles about N,N'-bis(3-tert-butyl-5-methoxy-2-hydroxyphenylmethyl)-N,N'-dimethylethylenediamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 121-00-6,1341-82-8
3-tert-Butyl-4-hydroxyanisole

: 110-70-3
N,N`-dimethylethylenediamine

: 1305347-30-1
N,N'-bis(3-tert-butyl-5-methoxy-2-hydroxyphenylmethyl)-N,N'-dimethylethylenediamine

Guidance literature:: In water; for 48h; Reflux;
DOI:10.1016/j.ica.2012.10.015

Reference yield:

: 121-00-6,1341-82-8
3-tert-Butyl-4-hydroxyanisole

: 110-70-3
N,N`-dimethylethylenediamine

: 1305347-30-1
N,N'-bis(3-tert-butyl-5-methoxy-2-hydroxyphenylmethyl)-N,N'-dimethylethylenediamine

Guidance literature:: With formaldehyd;
DOI:10.1016/j.poly.2015.11.003

Reference yield: 85.0%

: 1305347-30-1
N,N'-bis(3-tert-butyl-5-methoxy-2-hydroxyphenylmethyl)-N,N'-dimethylethylenediamine

: 24356-01-2
tetrabenzylzirconium(IV)

: 1305347-19-6
[(N,N'-bis(3-tert-butyl-5-methoxy-2-hydroxyphenylmethyl)-N,N'-dimethylethylenediamine(-2H))Zr(CH₂Ph)2]

Guidance literature:: In toluene; under Ar; soln. of ligand in dry toluene added to soln. of Zr compd. in dry toluene; kept at 65°C for 2 h; modified from E. T. Tshuva, L.Goldberg, M. Kol, J. Am. Chem. Soc., 2000, 122(43), 10706; solvent removed under vac.; recrystd. from toluene-n-pentane; elem. anal.;
DOI:10.1021/om2001926