C₂₉H₃₆O₆S

Base Information

Chemical Name:C₂₉H₃₆O₆S
CAS No.:827325-54-2
Molecular Formula:C₂₉H₃₆O₆S
Molecular Weight:512.667
Hs Code.:

C<sub>29</sub>H<sub>36</sub>O<sub>6</sub>S

Synonyms:C₂₉H₃₆O₆S

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Chemical Property of C₂₉H₃₆O₆S

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Technology Process of C₂₉H₃₆O₆S

There total 19 articles about C₂₉H₃₆O₆S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

: C₂₉H₃₆O₆S

: 827325-54-2
C₂₉H₃₆O₆S

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; In benzene; for 4h; Heating;
DOI:10.1021/ja044123l

Reference yield: 47.0%

: 827325-52-0
C₂₉H₃₆O₆S

: 827325-54-2
C₂₉H₃₆O₆S

: C₂₉H₃₆O₆S

: C₂₉H₃₆O₆S

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; In benzene; for 5h; Heating;
DOI:10.1021/ja044123l

Reference yield:

: C₂₀H₃₀O₃

: 827325-54-2
C₂₉H₃₆O₆S

Guidance literature:: Multi-step reaction with 18 steps

1.1: 98 percent / KH / tetrahydrofuran / Heating

2.1: 76 percent / Hoveyda-Grubbs catalyst / toluene / 30 h / Heating

3.1: aq. HCl / tetrahydrofuran / 3 h / Heating

4.1: 1.9 g / NaBH₄ / ethanol; tetrahydrofuran / 0.25 h / 0 °C

5.1: PPh₃; imidazole; I₂ / tetrahydrofuran / 3 h / 0 °C

5.2: 94 percent / t-BuOK / tetrahydrofuran; dimethylsulfoxide / 20 °C

6.1: 49 percent / SeO₂; aq. AcOH; t-BuOOH / CH₂Cl₂; decane / 2 h / 20 °C

7.1: 74 percent / Dess-Martin periodinane / CH₂Cl₂ / 1.5 h / -40 - 10 °C

8.1: 74 percent / aq. RhCl₃ / aq. ethanol / 0.58 h / 115 °C

9.1: 94 percent / P(OMe)3; O₂; t-BuOK / tetrahydrofuran; 2-methyl-propan-2-ol / 0.75 h / -40 °C

10.1: 73 percent / VO(acac)2; t-BuOOH / benzene; decane / 10 h / 20 °C

11.1: 72 percent / Et₃N / CH₂Cl₂ / 1 h / -10 - -5 °C

12.1: NaBH₄ / methanol / 5 h / 20 °C

13.1: 39 mg / PPTS / CH₂Cl₂ / 0.5 h / Heating

14.1: 90 percent / 2,3-dichloro-5,6-dicyano-1,4-benzoquinone / CH₂Cl₂ / 18 h / 20 °C

15.1: 96 percent / Et₃N / CH₂Cl₂ / 0.75 h / -78 °C

16.1: 76 percent / Li₂CO₃ / dimethylformamide / 5 h / 55 °C

17.1: 97 percent / (NH₄)6Mo₇O₂₄; aq. H₂O₂ / aq. ethanol / 6 h / 20 °C

18.1: 47 percent / 1,8-diazabicyclo[5.4.0]undec-7-ene / benzene / 5 h / Heating

With 1H-imidazole; hydrogenchloride; tert.-butylhydroperoxide; [1,3-bis-(2,4,6-trimethylphenyl)-2-imidazolidinylidene]dichloro(O-isopropoxyphenylmethylene)ruthenium; ammonium heptamolybdate; sodium tetrahydroborate; rhodium(III) chloride; selenium(IV) oxide; bis(acetylacetonate)oxovanadium; potassium tert-butylate; dihydrogen peroxide; iodine; oxygen; pyridinium p-toluenesulfonate; potassium hydride; lithium carbonate; Dess-Martin periodane; acetic acid; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; triphenylphosphine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; phosphorous acid trimethyl ester; In tetrahydrofuran; methanol; decane; ethanol; dichloromethane; N,N-dimethyl-formamide; toluene; tert-butyl alcohol; benzene; 2.1: Grubbs reaction;
DOI:10.1021/ja044123l