tert-butyl (1-(4-(6-carbamoyl-3-phenylbenzofuran-2-yl)phenyl)cyclobutyl)carbamate

Base Information

Chemical Name:tert-butyl (1-(4-(6-carbamoyl-3-phenylbenzofuran-2-yl)phenyl)cyclobutyl)carbamate
CAS No.:1301610-43-4
Molecular Formula:C₃₀H₃₀N₂O₄
Molecular Weight:482.579
Hs Code.:

Synonyms:tert-butyl (1-(4-(6-carbamoyl-3-phenylbenzofuran-2-yl)phenyl)cyclobutyl)carbamate

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Chemical Property of tert-butyl (1-(4-(6-carbamoyl-3-phenylbenzofuran-2-yl)phenyl)cyclobutyl)carbamate

Chemical Property:

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Technology Process of tert-butyl (1-(4-(6-carbamoyl-3-phenylbenzofuran-2-yl)phenyl)cyclobutyl)carbamate

There total 6 articles about tert-butyl (1-(4-(6-carbamoyl-3-phenylbenzofuran-2-yl)phenyl)cyclobutyl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 1301610-94-5
tert-butyl (1-(4-(6-cyano-3-phenylbenzofuran-2-yl)phenyl)cyclobutyl)carbamate

: 1301610-43-4
tert-butyl (1-(4-(6-carbamoyl-3-phenylbenzofuran-2-yl)phenyl)cyclobutyl)carbamate

Guidance literature:: With water; dihydrogen peroxide; potassium carbonate; In dimethyl sulfoxide; at 30 - 70 ℃;

Reference yield:

: 1032350-06-3
tert-butyl (1-(4-bromophenyl)cyclobutyl)carbamate

: 1301610-43-4
tert-butyl (1-(4-(6-carbamoyl-3-phenylbenzofuran-2-yl)phenyl)cyclobutyl)carbamate

Guidance literature:: Multi-step reaction with 6 steps

1: diisopropylamine / copper(l) iodide; bis(tri-t-butylphosphine)palladium⁽⁰⁾ / 1,4-dioxane / 20 h / 20 - 80 °C / Inert atmosphere

2: potassium carbonate; methanol / 1 h

3: triethylamine / copper(l) iodide; bis(tri-t-butylphosphine)palladium⁽⁰⁾ / 18 h / 0 - 20 °C / Inert atmosphere

4: Iodine monochloride / dichloromethane / 0.5 h / 0 - 20 °C / Inert atmosphere

5: cesium fluoride / triphenylphosphine; palladium diacetate / 1,2-dimethoxyethane / 5 h / 75 °C

6: potassium carbonate; water; dihydrogen peroxide / dimethyl sulfoxide / 30 - 70 °C

With methanol; water; dihydrogen peroxide; Iodine monochloride; potassium carbonate; triethylamine; diisopropylamine; cesium fluoride; copper(l) iodide; bis(tri-t-butylphosphine)palladium⁽⁰⁾; palladium diacetate; triphenylphosphine; In 1,4-dioxane; 1,2-dimethoxyethane; dichloromethane; dimethyl sulfoxide;

Reference yield:

: 1301610-33-2
tert-butyl 1-(4-ethynylphenyl)cyclobutylcarbamate

: 1301610-43-4
tert-butyl (1-(4-(6-carbamoyl-3-phenylbenzofuran-2-yl)phenyl)cyclobutyl)carbamate

Guidance literature:: Multi-step reaction with 4 steps

1: triethylamine / copper(l) iodide; bis(tri-t-butylphosphine)palladium⁽⁰⁾ / 18 h / 0 - 20 °C / Inert atmosphere

2: Iodine monochloride / dichloromethane / 0.5 h / 0 - 20 °C / Inert atmosphere

3: cesium fluoride / triphenylphosphine; palladium diacetate / 1,2-dimethoxyethane / 5 h / 75 °C

4: potassium carbonate; water; dihydrogen peroxide / dimethyl sulfoxide / 30 - 70 °C

With water; dihydrogen peroxide; Iodine monochloride; potassium carbonate; triethylamine; cesium fluoride; copper(l) iodide; bis(tri-t-butylphosphine)palladium⁽⁰⁾; palladium diacetate; triphenylphosphine; In 1,2-dimethoxyethane; dichloromethane; dimethyl sulfoxide;