3-(2,4-Dibromo-phenyl)-2-[3-(2,4-dibromo-phenyl)-5-phenyl-3H-[1,3,4]thiadiazol-(2Z)-ylidenemethyl]-2-methyl-5-phenyl-2,3-dihydro-[1,3,4]thiadiazole

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Chemical Name:3-(2,4-Dibromo-phenyl)-2-[3-(2,4-dibromo-phenyl)-5-phenyl-3H-[1,3,4]thiadiazol-(2Z)-ylidenemethyl]-2-methyl-5-phenyl-2,3-dihydro-[1,3,4]thiadiazole
CAS No.:85921-07-9
Molecular Formula:C₃₀H₂₀Br₄N₄S₂
Molecular Weight:820.264
Hs Code.:

Synonyms:3-(2,4-Dibromo-phenyl)-2-[3-(2,4-dibromo-phenyl)-5-phenyl-3H-[1,3,4]thiadiazol-(2Z)-ylidenemethyl]-2-methyl-5-phenyl-2,3-dihydro-[1,3,4]thiadiazole

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Chemical Property of 3-(2,4-Dibromo-phenyl)-2-[3-(2,4-dibromo-phenyl)-5-phenyl-3H-[1,3,4]thiadiazol-(2Z)-ylidenemethyl]-2-methyl-5-phenyl-2,3-dihydro-[1,3,4]thiadiazole

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Technology Process of 3-(2,4-Dibromo-phenyl)-2-[3-(2,4-dibromo-phenyl)-5-phenyl-3H-[1,3,4]thiadiazol-(2Z)-ylidenemethyl]-2-methyl-5-phenyl-2,3-dihydro-[1,3,4]thiadiazole

There total 3 articles about 3-(2,4-Dibromo-phenyl)-2-[3-(2,4-dibromo-phenyl)-5-phenyl-3H-[1,3,4]thiadiazol-(2Z)-ylidenemethyl]-2-methyl-5-phenyl-2,3-dihydro-[1,3,4]thiadiazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 3-(2,4-dibromophenyl)-2-methyl-5-phenyl-1,3,4-thiadiazolium perchlorate

: 85921-07-9
3-(2,4-Dibromo-phenyl)-2-[3-(2,4-dibromo-phenyl)-5-phenyl-3H-[1,3,4]thiadiazol-(2Z)-ylidenemethyl]-2-methyl-5-phenyl-2,3-dihydro-[1,3,4]thiadiazole

Guidance literature:: With triethylamine; In acetonitrile; for 0.5h;

Reference yield:

: 57279-86-4
N'-acetyl-N'-(2,4-dibromophenyl)benzothiohydrazide

: 85921-07-9
3-(2,4-Dibromo-phenyl)-2-[3-(2,4-dibromo-phenyl)-5-phenyl-3H-[1,3,4]thiadiazol-(2Z)-ylidenemethyl]-2-methyl-5-phenyl-2,3-dihydro-[1,3,4]thiadiazole

Guidance literature:: Multi-step reaction with 2 steps

1: 88 percent / perchloric acid / acetic anhydride

2: 81 percent / triethylamine / acetonitrile / 0.5 h

With perchloric acid; triethylamine; In acetic anhydride; acetonitrile;

Reference yield:

: 52215-24-4
N'-(2,4-dibromophenyl)benzothiohydrazide

: 85921-07-9
3-(2,4-Dibromo-phenyl)-2-[3-(2,4-dibromo-phenyl)-5-phenyl-3H-[1,3,4]thiadiazol-(2Z)-ylidenemethyl]-2-methyl-5-phenyl-2,3-dihydro-[1,3,4]thiadiazole

Guidance literature:: Multi-step reaction with 2 steps

1: 77 percent / perchloric acid / acetic acid / 0.08 h / Heating

2: 81 percent / triethylamine / acetonitrile / 0.5 h

With perchloric acid; triethylamine; In acetic acid; acetonitrile;