bis(triphenylphosphine)(acetylacetonato)palladium(II) hexafluorophosphate-acetone (1/1)

Base Information

Chemical Name:bis(triphenylphosphine)(acetylacetonato)palladium(II) hexafluorophosphate-acetone (1/1)
CAS No.:80583-70-6
Molecular Formula:C₃H₆O*C₄₁H₃₇O₂P₂Pd*F₆P
Molecular Weight:933.155
Hs Code.:

Synonyms:bis(triphenylphosphine)(acetylacetonato)palladium(II) hexafluorophosphate-acetone (1/1)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of bis(triphenylphosphine)(acetylacetonato)palladium(II) hexafluorophosphate-acetone (1/1)

Chemical Property:

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Technology Process of bis(triphenylphosphine)(acetylacetonato)palladium(II) hexafluorophosphate-acetone (1/1)

There total 3 articles about bis(triphenylphosphine)(acetylacetonato)palladium(II) hexafluorophosphate-acetone (1/1) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 14221-01-3
tetrakis(triphenylphosphine) palladium⁽⁰⁾

: 437-17-2
tritylium hexafluorophosphate

: 123-54-6,81235-32-7
acetylacetone

: 80583-70-6
bis(triphenylphosphine)(acetylacetonato)palladium(II) hexafluorophosphate-acetone (1/1)

Guidance literature:: With acetone; In dichloromethane; benzene; (N2); CPh3PF6 oxidation of the Pd complex in benzene-CH2Cl2 containing acetylacetone at room temp. for 24 h; recrystn. from acetone-ether; elem. anal.;
DOI:10.1021/ic00134a072

Reference yield:

: 80583-64-8
tetrakis(triphenylphosphine)palladium(II) hexafluorophosphate-acetone (1/1)

: 1118-67-8
sodium (Z)-4-oxopent-2-en-2-olate

: 80583-70-6
bis(triphenylphosphine)(acetylacetonato)palladium(II) hexafluorophosphate-acetone (1/1)

Guidance literature:: In ethanol; acetone; reaction of equimolar amounts in warmed CH3OH-acetone; elem. anal.;
DOI:10.1021/ic00134a072

Reference yield:

: 17084-13-8
potassium hexafluorophosphate

: bis(acetylacetonato)palladium(II)

: 603-35-0
triphenylphosphine

: 80583-70-6
Pd(CH₃COCHCOCH₃)(P(C₆H₅)3)2⁽¹⁺⁾*PF₆^(1-)=[Pd(CH₃COCHCOCH₃)(P(C₆H₅)3)2]PF₆

Guidance literature:: In methanol; stirring Pt-complex with 2 equiv. PPh3, addn. of equimolar amt. of KPF6 (pptn.); recrystn. (CH2Cl2/pentane), filtration;
DOI:10.1016/S0022-328X(97)00432-4