tetrakis(triphenylphosphine)palladium(II) hexafluorophosphate-acetone (1/1)

Base Information

Chemical Name:tetrakis(triphenylphosphine)palladium(II) hexafluorophosphate-acetone (1/1)
CAS No.:80583-64-8
Molecular Formula:C₃H₆O*C₇₂H₆₀P₄Pd*2F₆P
Molecular Weight:1503.59
Hs Code.:

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Chemical Property of tetrakis(triphenylphosphine)palladium(II) hexafluorophosphate-acetone (1/1)

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Technology Process of tetrakis(triphenylphosphine)palladium(II) hexafluorophosphate-acetone (1/1)

There total 1 articles about tetrakis(triphenylphosphine)palladium(II) hexafluorophosphate-acetone (1/1) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 14221-01-3
tetrakis(triphenylphosphine) palladium⁽⁰⁾

: 437-17-2
tritylium hexafluorophosphate

: 80583-64-8
tetrakis(triphenylphosphine)palladium(II) hexafluorophosphate-acetone (1/1)

: 17854-07-8
hexaphenylethane

Guidance literature:: In acetone; benzene; (N2); an acetone soln. of CPh3PF6 was added to a benzene soln. of the Pd complex, the mixed soln. was left agitating for 6 h; reduced in vol., Et2O was added; elem. anal.;
DOI:10.1021/ic00134a072

Reference yield: 57.0%

: 80583-64-8
tetrakis(triphenylphosphine)palladium(II) hexafluorophosphate-acetone (1/1)

: chlorotris(triphenylphosphine)palladium(II) hexafluorophosphate * acetone

Guidance literature:: With t-BuCl; In dichloromethane; acetone; to suspn. of Pd complex in acetone soln. of t-BuCl in CH2Cl2 was added,mixt. was stirred overnight; soln. was filtered, reduced in vac., pptd. with ether, ppt. was recrystd. from acetone with equimolar quantity of PPh3, elem. anal.;
DOI:10.1016/S0277-5387(00)86711-X

Reference yield: 55.0%

: 66-71-7
1,10-Phenanthroline

: 80583-64-8
tetrakis(triphenylphosphine)palladium(II) hexafluorophosphate-acetone (1/1)

: 80583-69-3
bis(1,10-phenanthroline)(triphenylphosphine)palladium(II) hexafluorophosphate-acetone (1/1)

Guidance literature:: In acetone; (N2); phenanthroline was added to a soln. of the Pd complex in acetone; evapd., recrystd. from acetone-ether; elem. anal.;
DOI:10.1021/ic00134a072