3-(5-(4-((4-(diphenylamino)phenyl)ethynyl)phenyl)thiophen-2-yl)-2,5-dioctyl-6-(thiophen-2-yl)-2,3,5,6-tetrahydropyrrolo[3,4-c]pyrrole-1,4-dione

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Chemical Name:3-(5-(4-((4-(diphenylamino)phenyl)ethynyl)phenyl)thiophen-2-yl)-2,5-dioctyl-6-(thiophen-2-yl)-2,3,5,6-tetrahydropyrrolo[3,4-c]pyrrole-1,4-dione
CAS No.:1620996-84-0
Molecular Formula:C₅₆H₅₇N₃O₂S₂
Molecular Weight:868.219
Hs Code.:

Synonyms:3-(5-(4-((4-(diphenylamino)phenyl)ethynyl)phenyl)thiophen-2-yl)-2,5-dioctyl-6-(thiophen-2-yl)-2,3,5,6-tetrahydropyrrolo[3,4-c]pyrrole-1,4-dione

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Chemical Property of 3-(5-(4-((4-(diphenylamino)phenyl)ethynyl)phenyl)thiophen-2-yl)-2,5-dioctyl-6-(thiophen-2-yl)-2,3,5,6-tetrahydropyrrolo[3,4-c]pyrrole-1,4-dione

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Technology Process of 3-(5-(4-((4-(diphenylamino)phenyl)ethynyl)phenyl)thiophen-2-yl)-2,5-dioctyl-6-(thiophen-2-yl)-2,3,5,6-tetrahydropyrrolo[3,4-c]pyrrole-1,4-dione

There total 9 articles about 3-(5-(4-((4-(diphenylamino)phenyl)ethynyl)phenyl)thiophen-2-yl)-2,5-dioctyl-6-(thiophen-2-yl)-2,3,5,6-tetrahydropyrrolo[3,4-c]pyrrole-1,4-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 1335015-92-3
3-(5-bromo-thiophen-2-yl)-2,5-dioctyl-6-(thiophen-2-yl)-2,3,5,6-tetrahydropyrrolo[3,4-c]pyrrole-1,4-dione

: 1607819-42-0
N-{4-[4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)phenyl]ethynylphenyl}diphenylamine

: 1620996-84-0
3-(5-(4-((4-(diphenylamino)phenyl)ethynyl)phenyl)thiophen-2-yl)-2,5-dioctyl-6-(thiophen-2-yl)-2,3,5,6-tetrahydropyrrolo[3,4-c]pyrrole-1,4-dione

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; In ethanol; water; toluene; at 110 ℃; for 12h; Inert atmosphere; Schlenk technique;
DOI:10.1039/c4cc04020a

Reference yield:

: 3,6-dithiophen-2-yl-2,5-dihydropyrrolo[3,4-c]pyrrole-1,4-dione

: 1620996-84-0
3-(5-(4-((4-(diphenylamino)phenyl)ethynyl)phenyl)thiophen-2-yl)-2,5-dioctyl-6-(thiophen-2-yl)-2,3,5,6-tetrahydropyrrolo[3,4-c]pyrrole-1,4-dione

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 1 h / 60 °C / Inert atmosphere; Schlenk technique

1.2: 18 h / 60 °C / Inert atmosphere; Schlenk technique

2.1: N-Bromosuccinimide / chloroform / 20 °C / Inert atmosphere; Schlenk technique

3.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / toluene; water; ethanol / 12 h / 110 °C / Inert atmosphere; Schlenk technique

With N-Bromosuccinimide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; potassium carbonate; In ethanol; chloroform; water; N,N-dimethyl-formamide; toluene; 3.1: |Suzuki Coupling;
DOI:10.1039/c4cc04020a

Reference yield:

: 1003-31-2
thiophene-2-carbonitrile

: 1620996-84-0
3-(5-(4-((4-(diphenylamino)phenyl)ethynyl)phenyl)thiophen-2-yl)-2,5-dioctyl-6-(thiophen-2-yl)-2,3,5,6-tetrahydropyrrolo[3,4-c]pyrrole-1,4-dione

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium; iron(III) chloride / tert-Amyl alcohol / 24 h / 120 °C / Inert atmosphere; Schlenk technique

2.1: potassium carbonate / N,N-dimethyl-formamide / 1 h / 60 °C / Inert atmosphere; Schlenk technique

2.2: 18 h / 60 °C / Inert atmosphere; Schlenk technique

3.1: N-Bromosuccinimide / chloroform / 20 °C / Inert atmosphere; Schlenk technique

4.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / toluene; water; ethanol / 12 h / 110 °C / Inert atmosphere; Schlenk technique

With iron(III) chloride; N-Bromosuccinimide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium; sodium carbonate; potassium carbonate; In tert-Amyl alcohol; ethanol; chloroform; water; N,N-dimethyl-formamide; toluene; 4.1: |Suzuki Coupling;
DOI:10.1039/c4cc04020a