N-{4-[4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)phenyl]ethynylphenyl}diphenylamine

Base Information

Chemical Name:N-{4-[4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)phenyl]ethynylphenyl}diphenylamine
CAS No.:1607819-42-0
Molecular Formula:C₃₂H₃₀BNO₂
Molecular Weight:471.407
Hs Code.:

Synonyms:N-{4-[4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)phenyl]ethynylphenyl}diphenylamine

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Chemical Property of N-{4-[4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)phenyl]ethynylphenyl}diphenylamine

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Technology Process of N-{4-[4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)phenyl]ethynylphenyl}diphenylamine

There total 7 articles about N-{4-[4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)phenyl]ethynylphenyl}diphenylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 1209009-14-2
N-{4-[2-(4-bromophenyl)ethynyl]phenyl}diphenylamine

: 73183-34-3
bis(pinacol)diborane

: 1607819-42-0
N-{4-[4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)phenyl]ethynylphenyl}diphenylamine

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; potassium acetate; triphenylphosphine; In toluene; at 110 ℃; for 24h; Inert atmosphere; Schlenk technique;
DOI:10.1039/c4cc04020a

Reference yield:

: 589-87-7
1,4-bromoiodobenzene

: 205877-26-5
4-diphenylaminophenylacetylene

: 1-(4-bromo-phenyl)-1-decyne

: 1607819-42-0
N-{4-[4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)phenyl]ethynylphenyl}diphenylamine

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene / Reflux

2: potassium acetate; bis-triphenylphosphine-palladium(II) chloride; triphenylphosphine / toluene / Reflux

With bis-triphenylphosphine-palladium(II) chloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium acetate; potassium carbonate; triphenylphosphine; In toluene; 1: |Suzuki Coupling / 2: |Miyaura Borylation Reaction;
DOI:10.1039/c3tc32214a

Reference yield:

: 589-87-7
1,4-bromoiodobenzene

: 205877-26-5
4-diphenylaminophenylacetylene

: 1-(4-bromo-phenyl)-1-decyne

: 1607819-42-0
N-{4-[4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)phenyl]ethynylphenyl}diphenylamine

: 1,4-bis(4-(pyrrolidin-1-yl)piperidin-1-yl)benzene trifluoroacetate

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene / Reflux

2: potassium acetate; bis-triphenylphosphine-palladium(II) chloride; triphenylphosphine / toluene / Reflux

With bis-triphenylphosphine-palladium(II) chloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium acetate; potassium carbonate; triphenylphosphine; In toluene; 1: |Suzuki Coupling / 2: |Miyaura Borylation Reaction;
DOI:10.1039/c3tc32214a