1-phenyl-octahydro-1-phospha-2,3-cyclo-dicyclopropa[a,cd]pentalene 1-oxide

Base Information

• Chemical Name: 1-phenyl-octahydro-1-phospha-2,3-cyclo-dicyclopropa[a,cd]pentalene 1-oxide
• CAS No.: 43017-31-8
• Molecular Formula: C₁₄H₁₃OP
• Molecular Weight: 228.23

Synonyms:1-phenyl-octahydro-1-phospha-2,3-cyclo-dicyclopropa[a,cd]pentalene 1-oxide

Chemical Property of 1-phenyl-octahydro-1-phospha-2,3-cyclo-dicyclopropa[a,cd]pentalene 1-oxide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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Technology Process of 1-phenyl-octahydro-1-phospha-2,3-cyclo-dicyclopropa[a,cd]pentalene 1-oxide

There total 7 articles about 1-phenyl-octahydro-1-phospha-2,3-cyclo-dicyclopropa[a,cd]pentalene 1-oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Dichlorophenylphosphine (644-97-3) → 1-phenyl-octahydro-1-phospha-2,3-cyclo-dicyclopropa[a,cd]pentalene 1-oxide (43017-31-8)

Guidance literature:

Multi-step reaction with 6 steps

1: (i) Li, Et₂O, (ii) /BRN= 508189/, (iii) H₂O

2: Heating

3: H₂O₂ / CHCl₃; H₂O

4: benzene / Irradiation

5: benzene; acetone / Irradiation

6: AgBF₄ / CHCl₃

With silver tetrafluoroborate; dihydrogen peroxide; In chloroform; water; acetone; benzene;

DOI:10.1021/ja00794a027

Reference yield:

1,3,5,7-cyclooctatetraene (629-20-9) → 1-phenyl-octahydro-1-phospha-2,3-cyclo-dicyclopropa[a,cd]pentalene 1-oxide (43017-31-8)

Guidance literature:

Multi-step reaction with 5 steps

1: (i) Li, Et₂O, (ii) /BRN= 508189/, (iii) H₂O

2: Heating

3: H₂O₂ / CHCl₃; H₂O

4: benzene; acetone / Irradiation

5: AgBF₄ / CHCl₃

With silver tetrafluoroborate; dihydrogen peroxide; In chloroform; water; acetone; benzene;

DOI:10.1021/ja00794a027

Reference yield:

anti-9-phenyl-9-phosphabicyclo<4.2.1>nona-2,4,7-trien (13887-07-5) → 1-phenyl-octahydro-1-phospha-2,3-cyclo-dicyclopropa[a,cd]pentalene 1-oxide (43017-31-8)

Guidance literature:

Multi-step reaction with 4 steps

1: H₂O₂ / CHCl₃; H₂O

2: benzene / Irradiation

3: benzene; acetone / Irradiation

4: AgBF₄ / CHCl₃

With silver tetrafluoroborate; dihydrogen peroxide; In chloroform; water; acetone; benzene;

DOI:10.1021/ja00794a027

upstream raw materials:

9-phenyl-9-phospha-pentacyclo[4.3.0.0^2,5.0^3,8.0^4,7]nonane 9-oxide

1,3,5,7-cyclooctatetraene

anti-9-phenyl-9-phosphatricyclo<4.2.1.0^2,5>nona-3,7-diene-9-oxide

Dichlorophenylphosphine

Downstream raw materials:

(2-phenylethyl)diphenylphosphine oxide

1-methyl-1-phenyl-octahydro-1-phospha-2,3-cyclo-dicyclopropa[a,cd]pentalenium; iodide

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