(S)-3-cyano-3,3-diphenylpropyl 4-(5-(5-amino-4-(2-(bis(ethylthio)methyl)pyrrolidine-1-carbonyl)-2-methoxyphenoxy)pentyl)piperazine-1-carbodithioate

Base Information

Chemical Name:(S)-3-cyano-3,3-diphenylpropyl 4-(5-(5-amino-4-(2-(bis(ethylthio)methyl)pyrrolidine-1-carbonyl)-2-methoxyphenoxy)pentyl)piperazine-1-carbodithioate
CAS No.:1227458-42-5
Molecular Formula:C₄₃H₅₇N₅O₃S₄
Molecular Weight:820.221
Hs Code.:

(S)-3-cyano-3,3-diphenylpropyl 4-(5-(5-amino-4-(2-(bis(ethylthio)methyl)pyrrolidine-1-carbonyl)-2-methoxyphenoxy)pentyl)piperazine-1-carbodithioate

Synonyms:(S)-3-cyano-3,3-diphenylpropyl 4-(5-(5-amino-4-(2-(bis(ethylthio)methyl)pyrrolidine-1-carbonyl)-2-methoxyphenoxy)pentyl)piperazine-1-carbodithioate

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Chemical Property of (S)-3-cyano-3,3-diphenylpropyl 4-(5-(5-amino-4-(2-(bis(ethylthio)methyl)pyrrolidine-1-carbonyl)-2-methoxyphenoxy)pentyl)piperazine-1-carbodithioate

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Technology Process of (S)-3-cyano-3,3-diphenylpropyl 4-(5-(5-amino-4-(2-(bis(ethylthio)methyl)pyrrolidine-1-carbonyl)-2-methoxyphenoxy)pentyl)piperazine-1-carbodithioate

There total 5 articles about (S)-3-cyano-3,3-diphenylpropyl 4-(5-(5-amino-4-(2-(bis(ethylthio)methyl)pyrrolidine-1-carbonyl)-2-methoxyphenoxy)pentyl)piperazine-1-carbodithioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 1227458-41-4
(S)-3-cyano-3,3-diphenylpropyl 4-(5-(4-(2-(bis(ethylthio)methyl)pyrrolidine-1-carbonyl)-2-methoxy-5-nitrophenoxy)pentyl)piperazine-1-carbodithioate

: 1227458-42-5
(S)-3-cyano-3,3-diphenylpropyl 4-(5-(5-amino-4-(2-(bis(ethylthio)methyl)pyrrolidine-1-carbonyl)-2-methoxyphenoxy)pentyl)piperazine-1-carbodithioate

Guidance literature:: With tin(II) chloride dihdyrate; In methanol; Reflux;
DOI:10.1016/j.bioorg.2015.01.002

Reference yield:

: 897932-88-6
3-cyano-3,3-diphenylpropylpiperazine-1-carbodithioate

: 1227458-42-5
(S)-3-cyano-3,3-diphenylpropyl 4-(5-(5-amino-4-(2-(bis(ethylthio)methyl)pyrrolidine-1-carbonyl)-2-methoxyphenoxy)pentyl)piperazine-1-carbodithioate

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 48 h / 20 °C

2.1: tin(II) chloride hydrate / methanol / 5 h / Reflux

2.2: pH 8

With tin(II) chloride hydrate; potassium carbonate; In methanol; N,N-dimethyl-formamide;

Reference yield:

: 343308-57-6
(2S)-N-[4-(5-bromopentyloxy)-5-methoxy-2-nitrobenzoyl]pyrrolidine-2-carboxaldehyde diethyl thioacetal

: 1227458-42-5
(S)-3-cyano-3,3-diphenylpropyl 4-(5-(5-amino-4-(2-(bis(ethylthio)methyl)pyrrolidine-1-carbonyl)-2-methoxyphenoxy)pentyl)piperazine-1-carbodithioate

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 48 h / 20 °C

2.1: tin(II) chloride hydrate / methanol / 5 h / Reflux

2.2: pH 8

With tin(II) chloride hydrate; potassium carbonate; In methanol; N,N-dimethyl-formamide;