2'-(4-dimethylaminobenzylidene)-2-hydroxybenzoylhydrazide

Base Information

Chemical Name:2'-(4-dimethylaminobenzylidene)-2-hydroxybenzoylhydrazide
CAS No.:87444-18-6
Molecular Formula:C₁₆H₁₇N₃O₂
Molecular Weight:283.33
Hs Code.:

Synonyms:2'-(4-dimethylaminobenzylidene)-2-hydroxybenzoylhydrazide

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Chemical Property of 2'-(4-dimethylaminobenzylidene)-2-hydroxybenzoylhydrazide

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Technology Process of 2'-(4-dimethylaminobenzylidene)-2-hydroxybenzoylhydrazide

There total 1 articles about 2'-(4-dimethylaminobenzylidene)-2-hydroxybenzoylhydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 87444-18-6
2'-(4-dimethylaminobenzylidene)-2-hydroxybenzoylhydrazide

Guidance literature:: /BRN= 3365914/;
DOI:10.1039/jr9500001582

Reference yield:

: 87444-18-6
2'-(4-dimethylaminobenzylidene)-2-hydroxybenzoylhydrazide

: 936-02-7
2-Hydroxybenzoylhydrazine

: 100-10-7
4-dimethylamino-benzaldehyde

Guidance literature:: With ethanol-acidic buffer; Rate constant; Thermodynamic data; -ΔG(excit.), ΔH(excit.),-ΔS(excit), E_a(excit.);
DOI:10.1039/P29840000337

Reference yield:

: nickel(II) chloride hexahydrate

: 87444-18-6
2'-(4-dimethylaminobenzylidene)-2-hydroxybenzoylhydrazide

: [NiCl(H₂O)(C₆H₄(OH)C(O)N(H)NCHC₆H₄(N(CH₃)2))2]⁽¹⁺⁾*Cl^(1-)*2H₂O=[NiCl(H₂O)(C₆H₄(OH)C(O)N(H)NCHC₆H₄(N(CH₃)2))2]Cl*2H₂O

Guidance literature:: In methanol; soln. of ligand mixed with Ni-compd., refluxed for 4-6 h; concd., digested on a water bath for 2 h, cooled to room temp., filtered, washed (MeOH), dried (P2O5); elem. anal.;