3-[1-(4,5-dihydro-1H-imidazol-2-yl)-3-hydroxypropoxy]-2-methylbenzenamine

Base Information

Chemical Name:3-[1-(4,5-dihydro-1H-imidazol-2-yl)-3-hydroxypropoxy]-2-methylbenzenamine
CAS No.:97817-80-6
Molecular Formula:C₁₃H₁₉N₃O₂
Molecular Weight:249.313
Hs Code.:

Synonyms:3-[1-(4,5-dihydro-1H-imidazol-2-yl)-3-hydroxypropoxy]-2-methylbenzenamine

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Chemical Property of 3-[1-(4,5-dihydro-1H-imidazol-2-yl)-3-hydroxypropoxy]-2-methylbenzenamine

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Technology Process of 3-[1-(4,5-dihydro-1H-imidazol-2-yl)-3-hydroxypropoxy]-2-methylbenzenamine

There total 3 articles about 3-[1-(4,5-dihydro-1H-imidazol-2-yl)-3-hydroxypropoxy]-2-methylbenzenamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 97817-66-8
4,5-dihydro-2-[1-(2-methyl-3-nitrophenoxy)-3-hydroxypropyl]-1H-imidazole

: 97817-80-6
3-[1-(4,5-dihydro-1H-imidazol-2-yl)-3-hydroxypropoxy]-2-methylbenzenamine

Guidance literature:: With hydrogen; palladium on activated charcoal;
DOI:10.1021/jm00164a024

Reference yield:

: 5460-31-1
3-nitro-o-cresol

: 97817-80-6
3-[1-(4,5-dihydro-1H-imidazol-2-yl)-3-hydroxypropoxy]-2-methylbenzenamine

Guidance literature:: Multi-step reaction with 3 steps

1: 58 percent / K₂CO₃ / dimethylformamide / 18 h

2: 1.) AlMe₃ / 1.) toluene, 5 deg C, 15 min, 2.) reflux, 3 h

3: 86 percent / H₂ / 10percent Pd/C

With hydrogen; trimethylaluminum; potassium carbonate; palladium on activated charcoal; In N,N-dimethyl-formamide;
DOI:10.1021/jm00164a024

Reference yield:

: 97817-65-7
3-(2-methyl-3-nitrophenoxy)oxacyclopentan-2-one

: 97817-80-6
3-[1-(4,5-dihydro-1H-imidazol-2-yl)-3-hydroxypropoxy]-2-methylbenzenamine

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) AlMe₃ / 1.) toluene, 5 deg C, 15 min, 2.) reflux, 3 h

2: 86 percent / H₂ / 10percent Pd/C

With hydrogen; trimethylaluminum; palladium on activated charcoal;
DOI:10.1021/jm00164a024