1,8-bis[2-(4,4,4-trifluoro-1-hydroxy-3-oxobut-1-enyl)phenoxy]-3,6-dioxaoctane

Base Information

Chemical Name:1,8-bis[2-(4,4,4-trifluoro-1-hydroxy-3-oxobut-1-enyl)phenoxy]-3,6-dioxaoctane
CAS No.:1300635-77-1
Molecular Formula:C₂₆H₂₄F₆O₈
Molecular Weight:578.462
Hs Code.:

Synonyms:1,8-bis[2-(4,4,4-trifluoro-1-hydroxy-3-oxobut-1-enyl)phenoxy]-3,6-dioxaoctane

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Chemical Property of 1,8-bis[2-(4,4,4-trifluoro-1-hydroxy-3-oxobut-1-enyl)phenoxy]-3,6-dioxaoctane

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Technology Process of 1,8-bis[2-(4,4,4-trifluoro-1-hydroxy-3-oxobut-1-enyl)phenoxy]-3,6-dioxaoctane

There total 2 articles about 1,8-bis[2-(4,4,4-trifluoro-1-hydroxy-3-oxobut-1-enyl)phenoxy]-3,6-dioxaoctane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 383-63-1
ethyl trifluoroacetate,

: 1,1'-((((ethane-1,2-diylbis(oxy))bis(ethane-2,1-diyl))bis(oxy))bis(2,1-phenylene))bis(ethan-1-one)

: 1300635-77-1
1,8-bis[2-(4,4,4-trifluoro-1-hydroxy-3-oxobut-1-enyl)phenoxy]-3,6-dioxaoctane

Guidance literature:: ethyl trifluoroacetate,; 1,1'-((((ethane-1,2-diylbis(oxy))bis(ethane-2,1-diyl))bis(oxy))bis(2,1-phenylene))bis(ethan-1-one); With methanol; lithium hydride; In diethyl ether; hexane; at 20 ℃; for 6.5h; Reflux;

With hydrogenchloride; In water;
DOI:10.1007/s11172-010-0365-z

Reference yield:

: 118-93-4,104809-67-8
o-hydroxyacetophenone

: 112-26-5,27252-69-3
1,2-bis(2-chloroethoxy)ethane

: 1300635-77-1
1,8-bis[2-(4,4,4-trifluoro-1-hydroxy-3-oxobut-1-enyl)phenoxy]-3,6-dioxaoctane

Guidance literature:: Multi-step reaction with 2 steps

1: aluminum oxide; potassium hydroxide / N,N-dimethyl-formamide / 12 h / 100 °C

2: methanol; lithium hydride / diethyl ether; hexane / 6.5 h / 20 °C / Reflux

With methanol; aluminum oxide; lithium hydride; potassium hydroxide; In diethyl ether; hexane; N,N-dimethyl-formamide; 1: Williamson synthesis;
DOI:10.1007/s11172-010-0365-z