{4-[4-(tetrahydropyran-2-yloxymethyl)benzoyl]benzyl}nosylcarbamic acid allyl ester

Base Information

Chemical Name:{4-[4-(tetrahydropyran-2-yloxymethyl)benzoyl]benzyl}nosylcarbamic acid allyl ester
CAS No.:943601-34-1
Molecular Formula:C₃₀H₃₀N₂O₉S
Molecular Weight:594.642
Hs Code.:

Synonyms:{4-[4-(tetrahydropyran-2-yloxymethyl)benzoyl]benzyl}nosylcarbamic acid allyl ester

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Chemical Property of {4-[4-(tetrahydropyran-2-yloxymethyl)benzoyl]benzyl}nosylcarbamic acid allyl ester

Chemical Property:

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Technology Process of {4-[4-(tetrahydropyran-2-yloxymethyl)benzoyl]benzyl}nosylcarbamic acid allyl ester

There total 1 articles about {4-[4-(tetrahydropyran-2-yloxymethyl)benzoyl]benzyl}nosylcarbamic acid allyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 90916-29-3
N-allyloxycarbonyl-2-nitrobenzenesulfonamide

: 676461-72-6
(4-hydroxymethyl-phenyl)-[4-(tetrahydro-pyran-2-yloxymethyl)-phenyl]-methanone

: 943601-34-1
{4-[4-(tetrahydropyran-2-yloxymethyl)benzoyl]benzyl}nosylcarbamic acid allyl ester

Guidance literature:: With triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; toluene; at 20 ℃; for 0.25h;
DOI:10.1021/ol070376i

Reference yield:

: 943601-34-1
{4-[4-(tetrahydropyran-2-yloxymethyl)benzoyl]benzyl}nosylcarbamic acid allyl ester

: 943601-35-2
{4-[4-(hydroxymethyl)benzoyl]benzyl}nosylcarbamic acid allyl ester

Guidance literature:: With (+)-10-camphorsulfonic acid; In methanol; dichloromethane; at 20 ℃; for 6h;
DOI:10.1021/ol070376i

Reference yield:

: 943601-34-1
{4-[4-(tetrahydropyran-2-yloxymethyl)benzoyl]benzyl}nosylcarbamic acid allyl ester

: C₃₆H₃₂N₄O₁₃S₂

Guidance literature:: Multi-step reaction with 2 steps

1: 9.24 g / (+)-camphorsulfonic acid / methanol; CH₂Cl₂ / 6 h / 20 °C

2: 99 percent / triphenylphosphine; diethyl azodicarboxylate / tetrahydrofuran; toluene / 0.25 h / 20 °C

With (+)-10-camphorsulfonic acid; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; methanol; dichloromethane; toluene; 2: Mitsunobu reaction;
DOI:10.1021/ol070376i