1-(tert-Butoxycarbonylamino)-7-[hydroxy(2-tert-butyldimethylsilyloxy-3-methoxyphenyl)methyl]-1H-benzotriazole

Base Information

Chemical Name:1-(tert-Butoxycarbonylamino)-7-[hydroxy(2-tert-butyldimethylsilyloxy-3-methoxyphenyl)methyl]-1H-benzotriazole
CAS No.:215807-83-3
Molecular Formula:C₂₅H₃₆N₄O₅Si
Molecular Weight:500.67
Hs Code.:

Synonyms:1-(tert-Butoxycarbonylamino)-7-[hydroxy(2-tert-butyldimethylsilyloxy-3-methoxyphenyl)methyl]-1H-benzotriazole

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-(tert-Butoxycarbonylamino)-7-[hydroxy(2-tert-butyldimethylsilyloxy-3-methoxyphenyl)methyl]-1H-benzotriazole

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Technology Process of 1-(tert-Butoxycarbonylamino)-7-[hydroxy(2-tert-butyldimethylsilyloxy-3-methoxyphenyl)methyl]-1H-benzotriazole

There total 1 articles about 1-(tert-Butoxycarbonylamino)-7-[hydroxy(2-tert-butyldimethylsilyloxy-3-methoxyphenyl)methyl]-1H-benzotriazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 181707-16-4
1-(tert-Butoxycarbonylamino)-1H-benzotriazole

: 126357-82-2
2-((tert-butyldimethylsilyl)oxy)-3-methoxybenzaldehyde

: 215807-83-3
1-(tert-Butoxycarbonylamino)-7-[hydroxy(2-tert-butyldimethylsilyloxy-3-methoxyphenyl)methyl]-1H-benzotriazole

Guidance literature:: With n-butyllithium; cerium(III) chloride; Tetraethylene glycol dimethyl ether; In tetrahydrofuran; hexane;
DOI:10.1055/s-1998-1878

Reference yield: 83.0%

: 215807-83-3
1-(tert-Butoxycarbonylamino)-7-[hydroxy(2-tert-butyldimethylsilyloxy-3-methoxyphenyl)methyl]-1H-benzotriazole

: 215807-68-4
1-(tert-Butoxycarbonylamino)-7-[hydroxy(2-hydroxy-3-methoxyphenyl)methyl]-1H-benzotriazole

Guidance literature:: With pyridine hydrogenfluoride; In dichloromethane; at 20 ℃;
DOI:10.1055/s-1998-1878

Reference yield:

: 215807-83-3
1-(tert-Butoxycarbonylamino)-7-[hydroxy(2-tert-butyldimethylsilyloxy-3-methoxyphenyl)methyl]-1H-benzotriazole

: 215807-49-1
1-(tert-Butoxycarbonylamino)-7-[(2-hydroxy-3-methoxyphenyl)methyl]-1H-benzotriazole

Guidance literature:: Multi-step reaction with 2 steps

1: 83 percent / HF*pyridine / CH₂Cl₂ / 48 h

2: 87 percent / H₂ / 5 percent Pd/C / methanol / 4 h / 20 °C

With hydrogen; pyridine hydrogenfluoride; palladium on activated charcoal; In methanol; dichloromethane;
DOI:10.1039/b103834f