(4E,6E,10RS)-10-(tert-butyldiphenylsilanyloxy)-7-methyl-10-thiophen-2-yldeca-4,6-dienal

Base Information

Chemical Name:(4E,6E,10RS)-10-(tert-butyldiphenylsilanyloxy)-7-methyl-10-thiophen-2-yldeca-4,6-dienal
CAS No.:431990-56-6
Molecular Formula:C₃₁H₃₈O₂SSi
Molecular Weight:502.793
Hs Code.:

Synonyms:(4E,6E,10RS)-10-(tert-butyldiphenylsilanyloxy)-7-methyl-10-thiophen-2-yldeca-4,6-dienal

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Chemical Property of (4E,6E,10RS)-10-(tert-butyldiphenylsilanyloxy)-7-methyl-10-thiophen-2-yldeca-4,6-dienal

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Technology Process of (4E,6E,10RS)-10-(tert-butyldiphenylsilanyloxy)-7-methyl-10-thiophen-2-yldeca-4,6-dienal

There total 1 articles about (4E,6E,10RS)-10-(tert-butyldiphenylsilanyloxy)-7-methyl-10-thiophen-2-yldeca-4,6-dienal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 431981-73-6
(4E,6E,10RS)-10-(tert-butyldiphenylsilanyloxy)-7-methyl-10-thiophen-2-yldeca-4,6-dien-1-ol

: 431990-56-6
(4E,6E,10RS)-10-(tert-butyldiphenylsilanyloxy)-7-methyl-10-thiophen-2-yldeca-4,6-dienal

Guidance literature:: With silica gel; pyridinium chlorochromate; In dichloromethane; for 1.5h;
DOI:10.1021/jm0105171

Reference yield:

: 134029-74-6
[(3,4,5-trimethoxyphenyl)methyl]phosphoric acid diethyl ester

: 431990-56-6
(4E,6E,10RS)-10-(tert-butyldiphenylsilanyloxy)-7-methyl-10-thiophen-2-yldeca-4,6-dienal

: tert-butyl-[(1RS,4E,6E,10Z)-4-methyl-1-thiophen-2-yl-11-(3,4,5-trimethoxyphenyl)undeca-4,6,10-trienyloxy]diphenylsilane

: tert-butyl-[(1RS,4E,6E,10E)-4-methyl-1-thiophen-2-yl-11-(3,4,5-trimethoxyphenyl)undeca-4,6,10-trienyloxy]diphenylsilane

Guidance literature:: [(3,4,5-trimethoxyphenyl)methyl]phosphoric acid diethyl ester; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 0.5h;

(4E,6E,10RS)-10-(tert-butyldiphenylsilanyloxy)-7-methyl-10-thiophen-2-yldeca-4,6-dienal; In tetrahydrofuran; hexane; at 20 ℃; for 1h; Further stages. Title compound not separated from byproducts.;
DOI:10.1021/jm0105171