(1R,2S)-1-((1R,2R,3R)-(4-(benzyloxy)-2-[(4-methoxybenzyl)oxy]-1,3-dimethyl)butyl)-2-methyl-4-pentenyl (methylsulfanyl)methanethioate

Base Information

Chemical Name:(1R,2S)-1-((1R,2R,3R)-(4-(benzyloxy)-2-[(4-methoxybenzyl)oxy]-1,3-dimethyl)butyl)-2-methyl-4-pentenyl (methylsulfanyl)methanethioate
CAS No.:1201638-83-6
Molecular Formula:C₂₉H₄₀O₄S₂
Molecular Weight:516.766
Hs Code.:

Synonyms:(1R,2S)-1-((1R,2R,3R)-(4-(benzyloxy)-2-[(4-methoxybenzyl)oxy]-1,3-dimethyl)butyl)-2-methyl-4-pentenyl (methylsulfanyl)methanethioate

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Chemical Property of (1R,2S)-1-((1R,2R,3R)-(4-(benzyloxy)-2-[(4-methoxybenzyl)oxy]-1,3-dimethyl)butyl)-2-methyl-4-pentenyl (methylsulfanyl)methanethioate

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Technology Process of (1R,2S)-1-((1R,2R,3R)-(4-(benzyloxy)-2-[(4-methoxybenzyl)oxy]-1,3-dimethyl)butyl)-2-methyl-4-pentenyl (methylsulfanyl)methanethioate

There total 1 articles about (1R,2S)-1-((1R,2R,3R)-(4-(benzyloxy)-2-[(4-methoxybenzyl)oxy]-1,3-dimethyl)butyl)-2-methyl-4-pentenyl (methylsulfanyl)methanethioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 75-15-0,12122-00-8
carbon disulfide

: 1201638-82-5
(4S,5R,6S,7R,8R)-9-(benzyloxy)-7-[(4-methoxybenzyl)oxy]-4,6,8-trimethyl-1-nonen-5-ol

: 74-88-4
methyl iodide

: 1201638-83-6
(1R,2S)-1-((1R,2R,3R)-(4-(benzyloxy)-2-[(4-methoxybenzyl)oxy]-1,3-dimethyl)butyl)-2-methyl-4-pentenyl (methylsulfanyl)methanethioate

Guidance literature:: (4S,5R,6S,7R,8R)-9-(benzyloxy)-7-[(4-methoxybenzyl)oxy]-4,6,8-trimethyl-1-nonen-5-ol; With sodium hydride; In tetrahydrofuran; at 0 - 25 ℃;

carbon disulfide; methyl iodide; In tetrahydrofuran; at 0 - 25 ℃;
DOI:10.1016/j.tetasy.2009.08.021

Reference yield: 91.0%

: 1201638-83-6
(1R,2S)-1-((1R,2R,3R)-(4-(benzyloxy)-2-[(4-methoxybenzyl)oxy]-1,3-dimethyl)butyl)-2-methyl-4-pentenyl (methylsulfanyl)methanethioate

: 1201638-84-7
(4S,6S,7S,8R)-9-(benzyloxy)-7-[(4-methoxybenzyl)oxy]-4,6,8-trimethyl-1-nonene

Guidance literature:: With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In toluene; for 1h; Reflux;
DOI:10.1016/j.tetasy.2009.08.021