2-(1-piperidinocycloprop-1-yl)-5,5-dimethyl-3-oxocyclohex-1-en-1-yl acetate

Base Information

• Chemical Name: 2-(1-piperidinocycloprop-1-yl)-5,5-dimethyl-3-oxocyclohex-1-en-1-yl acetate
• CAS No.: 110174-72-6
• Molecular Formula: C₁₈H₂₇NO₃
• Molecular Weight: 305.417

Synonyms:2-(1-piperidinocycloprop-1-yl)-5,5-dimethyl-3-oxocyclohex-1-en-1-yl acetate

Chemical Property of 2-(1-piperidinocycloprop-1-yl)-5,5-dimethyl-3-oxocyclohex-1-en-1-yl acetate

Chemical Property:

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Technology Process of 2-(1-piperidinocycloprop-1-yl)-5,5-dimethyl-3-oxocyclohex-1-en-1-yl acetate

There total 1 articles about 2-(1-piperidinocycloprop-1-yl)-5,5-dimethyl-3-oxocyclohex-1-en-1-yl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

5,5-Dimethyl-2-<1-(1-piperidinio)-cyclopropyl>-1-oxo-2-cyclohexen-3-olat (110174-70-4) + acetyl chloride (75-36-5) → 2-(1-piperidinocycloprop-1-yl)-5,5-dimethyl-3-oxocyclohex-1-en-1-yl acetate (110174-72-6)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In dichloromethane;

Reference yield: 70.0%

phenyl isocyanate (1197040-29-1,931-54-4) + 2-(1-piperidinocycloprop-1-yl)-5,5-dimethyl-3-oxocyclohex-1-en-1-yl acetate (110174-72-6) → C18H19NO2 (132292-34-3)

Guidance literature:

In dichloromethane; at 20 ℃; for 24h;

DOI:10.1055/s-1990-27073

Reference yield: 66.0%

2-(1-piperidinocycloprop-1-yl)-5,5-dimethyl-3-oxocyclohex-1-en-1-yl acetate (110174-72-6) → 6,7-dihydro-6,6-dimethyl-3-<<1-(3-hydroxy-5,5-dimethyl-1-oxocyclohex-2-en-2-yl)cycloprop-1-yl>methyl>benzofuran-4(5H)-one (110174-75-9)

Guidance literature:

In chloroform; for 96h; Heating;

DOI:10.1021/jo00231a016

upstream raw materials:

5,5-Dimethyl-2-<1-(1-piperidinio)-cyclopropyl>-1-oxo-2-cyclohexen-3-olat

acetyl chloride

Downstream raw materials:

2-<1-(2-Hhydroxy-4,4-dimethyl-6-oxo-1-cyclohexen-1-yl)-cyclopropyl>-N-methyl-N-phenylacetamid

C₁₈H₁₉NO₂

5,6,7,8-Tetrahydro-7,7-dimethyl-2-(methylphenylamino)-3-phenylspiro-<4H-chromen-4,1'-cyclopropan>-5-on

9-<1-(3-hydroxy-5,5-dimethyl-1-oxocyclohex-2-en-2-yl)cycloprop-1-yl>-3,4,6,7,8,9-hexahydro-3,3-dimethyldibenzofuran-1(2H)-one

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