7-chloro-9-methoxy-5,6-dihydro-[1,3]dioxolo[4',5':4,5]benzo[1,2-c]acridin-8-yl benzenesulfonate

Base Information

Chemical Name:7-chloro-9-methoxy-5,6-dihydro-[1,3]dioxolo[4',5':4,5]benzo[1,2-c]acridin-8-yl benzenesulfonate
CAS No.:1359946-06-7
Molecular Formula:C₂₅H₁₈ClNO₆S
Molecular Weight:495.94
Hs Code.:

Synonyms:7-chloro-9-methoxy-5,6-dihydro-[1,3]dioxolo[4',5':4,5]benzo[1,2-c]acridin-8-yl benzenesulfonate

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Chemical Property of 7-chloro-9-methoxy-5,6-dihydro-[1,3]dioxolo[4',5':4,5]benzo[1,2-c]acridin-8-yl benzenesulfonate

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Technology Process of 7-chloro-9-methoxy-5,6-dihydro-[1,3]dioxolo[4',5':4,5]benzo[1,2-c]acridin-8-yl benzenesulfonate

There total 5 articles about 7-chloro-9-methoxy-5,6-dihydro-[1,3]dioxolo[4',5':4,5]benzo[1,2-c]acridin-8-yl benzenesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 41303-45-1
6,7-methylenedioxy-1-tetralone

: 1359946-04-5
6-amino-3-methoxy-2-(phenylsulfonyloxy)benzoic acid

: 1359946-06-7
7-chloro-9-methoxy-5,6-dihydro-[1,3]dioxolo[4',5':4,5]benzo[1,2-c]acridin-8-yl benzenesulfonate

Guidance literature:: 6,7-methylenedioxy-1-tetralone; 6-amino-3-methoxy-2-(phenylsulfonyloxy)benzoic acid; With trichlorophosphate; for 8h; Reflux;

With sodium hydrogencarbonate; In dichloromethane; Saturated solution;
DOI:10.1016/j.ejmech.2012.03.034

Reference yield:

: 2426-60-0
2-Hydroxy-3-methoxy-6-nitrobenzaldehyde benzenesulfonate

: 1359946-06-7
7-chloro-9-methoxy-5,6-dihydro-[1,3]dioxolo[4',5':4,5]benzo[1,2-c]acridin-8-yl benzenesulfonate

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium permanganate / water; acetone / 2 h / 20 °C

2.1: iron; acetic acid / ethanol; water / 4 h / 20 °C

3.1: trichlorophosphate / 8 h / Reflux

3.2: Saturated solution

With potassium permanganate; iron; acetic acid; trichlorophosphate; In ethanol; water; acetone;
DOI:10.1016/j.ejmech.2012.03.034

Reference yield:

: 13575-74-1
4-(3,4-dimethoxyphenyl)butanoic acid

: 1359946-06-7
7-chloro-9-methoxy-5,6-dihydro-[1,3]dioxolo[4',5':4,5]benzo[1,2-c]acridin-8-yl benzenesulfonate

Guidance literature:: Multi-step reaction with 4 steps

1.1: polyphosphoric acid / dichloromethane / 2 h / Reflux

2.1: hydrogen bromide / 4 h / Reflux

3.1: potassium fluoride / N,N-dimethyl-formamide / 6 h / 140 °C

4.1: trichlorophosphate / 8 h / Reflux

4.2: Saturated solution

With potassium fluoride; hydrogen bromide; trichlorophosphate; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.ejmech.2012.03.034