3-isopropoxy-2-isopropylbenzenamine

Base Information

Chemical Name:3-isopropoxy-2-isopropylbenzenamine
CAS No.:1369935-68-1
Molecular Formula:C₁₂H₁₉NO
Molecular Weight:193.289
Hs Code.:

Synonyms:3-isopropoxy-2-isopropylbenzenamine

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Chemical Property of 3-isopropoxy-2-isopropylbenzenamine

Chemical Property:

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Technology Process of 3-isopropoxy-2-isopropylbenzenamine

There total 6 articles about 3-isopropoxy-2-isopropylbenzenamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,3-dimethoxybenzonitrile: 5653-62-3
2,3-dimethoxybenzonitrile

: 1369935-68-1
3-isopropoxy-2-isopropylbenzenamine

Guidance literature:: Multi-step reaction with 6 steps

1: diethyl ether / 0 - 20 °C / Inert atmosphere

2: aluminum tri-bromide; 1-thiopropane / dichloromethane / 0 - 20 °C / Inert atmosphere

3: caesium carbonate / acetonitrile / 24 h / 20 °C / Inert atmosphere

4: potassium carbonate; dihydrogen peroxide / dimethyl sulfoxide / 24 h / 0 - 20 °C

5: potassium hydroxide; [bis(acetoxy)iodo]benzene / 3.5 h / 0 - 25 °C / Inert atmosphere

6: lithium hydroxide / ethanol / 24 h / Reflux; Inert atmosphere

With aluminum tri-bromide; 1-thiopropane; [bis(acetoxy)iodo]benzene; dihydrogen peroxide; potassium carbonate; caesium carbonate; potassium hydroxide; lithium hydroxide; In diethyl ether; ethanol; dichloromethane; dimethyl sulfoxide; acetonitrile;
DOI:10.1021/ml3001775 DOI:10.1021/ml3001775

Reference yield:

: 1369819-67-9
3-isopropoxy-2-isopropylbenzonitrile

: 1369935-68-1
3-isopropoxy-2-isopropylbenzenamine

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate; dihydrogen peroxide / dimethyl sulfoxide / 24 h / 0 - 20 °C

2: potassium hydroxide; [bis(acetoxy)iodo]benzene / 3.5 h / 0 - 25 °C / Inert atmosphere

3: lithium hydroxide / ethanol / 24 h / Reflux; Inert atmosphere

With [bis(acetoxy)iodo]benzene; dihydrogen peroxide; potassium carbonate; potassium hydroxide; lithium hydroxide; In ethanol; dimethyl sulfoxide;
DOI:10.1021/ml3001775 DOI:10.1021/ml3001775

Reference yield:

: 1243279-74-4
3-hydroxy-2-isopropylbenzonitrile

: 1369935-68-1
3-isopropoxy-2-isopropylbenzenamine

Guidance literature:: Multi-step reaction with 4 steps

1: caesium carbonate / acetonitrile / 24 h / 20 °C / Inert atmosphere

2: potassium carbonate; dihydrogen peroxide / dimethyl sulfoxide / 24 h / 0 - 20 °C

3: potassium hydroxide; [bis(acetoxy)iodo]benzene / 3.5 h / 0 - 25 °C / Inert atmosphere

4: lithium hydroxide / ethanol / 24 h / Reflux; Inert atmosphere

With [bis(acetoxy)iodo]benzene; dihydrogen peroxide; potassium carbonate; caesium carbonate; potassium hydroxide; lithium hydroxide; In ethanol; dimethyl sulfoxide; acetonitrile;
DOI:10.1021/ml3001775 DOI:10.1021/ml3001775