2-benzoyl-1-benzyl-6,7-dimethoxy-1,2,3,4-tetrahydro-isoquinoline-1-carbonitrile

Base Information

Chemical Name:2-benzoyl-1-benzyl-6,7-dimethoxy-1,2,3,4-tetrahydro-isoquinoline-1-carbonitrile
CAS No.:25186-58-7
Molecular Formula:C₂₆H₂₄N₂O₃
Molecular Weight:412.488
Hs Code.:

Synonyms:2-benzoyl-1-benzyl-6,7-dimethoxy-1,2,3,4-tetrahydro-isoquinoline-1-carbonitrile

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Chemical Property of 2-benzoyl-1-benzyl-6,7-dimethoxy-1,2,3,4-tetrahydro-isoquinoline-1-carbonitrile

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Technology Process of 2-benzoyl-1-benzyl-6,7-dimethoxy-1,2,3,4-tetrahydro-isoquinoline-1-carbonitrile

There total 3 articles about 2-benzoyl-1-benzyl-6,7-dimethoxy-1,2,3,4-tetrahydro-isoquinoline-1-carbonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 100-44-7
benzyl chloride

: 10174-83-1
(±)-2-benzoyl-6,7-dimethoxy-1,2,3,4-tetrahydroisoquinoline-1-carbonitrile

: 25186-58-7
2-benzoyl-1-benzyl-6,7-dimethoxy-1,2,3,4-tetrahydro-isoquinoline-1-carbonitrile

Guidance literature:: With sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride; In dichloromethane; for 0.333333h; ultrasound sonication;

Reference yield:

: 3382-18-1
6,7-dimethoxy-3,4-dihydro-isoquinoline

: 25186-58-7
2-benzoyl-1-benzyl-6,7-dimethoxy-1,2,3,4-tetrahydro-isoquinoline-1-carbonitrile

Guidance literature:: Multi-step reaction with 2 steps

1: 42 percent / triethylbenzylammonmium chloride / CH₂Cl₂; H₂O / 0.33 h / Irradiation; ultrasound sonication

2: 90 percent / 50percent aq. NaOH / triethylbenzylammonium chloride / CH₂Cl₂ / 0.33 h / ultrasound sonication

With sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride; In dichloromethane; water;