11-methyl-8-(dimethylphenylsilyl)-7,11-diazatricyclo[7.3.1.0(2,7)]trideca-2,4-diene-6-one

Base Information

Chemical Name:11-methyl-8-(dimethylphenylsilyl)-7,11-diazatricyclo[7.3.1.0(2,7)]trideca-2,4-diene-6-one
CAS No.:1228275-14-6
Molecular Formula:C₂₀H₂₆N₂OSi
Molecular Weight:338.525
Hs Code.:

Synonyms:11-methyl-8-(dimethylphenylsilyl)-7,11-diazatricyclo[7.3.1.0(2,7)]trideca-2,4-diene-6-one

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Chemical Property of 11-methyl-8-(dimethylphenylsilyl)-7,11-diazatricyclo[7.3.1.0(2,7)]trideca-2,4-diene-6-one

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Technology Process of 11-methyl-8-(dimethylphenylsilyl)-7,11-diazatricyclo[7.3.1.0(2,7)]trideca-2,4-diene-6-one

There total 4 articles about 11-methyl-8-(dimethylphenylsilyl)-7,11-diazatricyclo[7.3.1.0(2,7)]trideca-2,4-diene-6-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 486-86-2
(-)-N-methylcystine

: 768-33-2
phenyldimethylsilyl chloride

: 1228275-14-6
11-methyl-8-(dimethylphenylsilyl)-7,11-diazatricyclo[7.3.1.0(2,7)]trideca-2,4-diene-6-one

Guidance literature:: With N,N,N,N,-tetramethylethylenediamine; lithium diisopropyl amide; In tetrahydrofuran; hexane; at -78 - 20 ℃;
DOI:10.1039/c8ob01456f

Reference yield: 13.0%

: 486-86-2
(-)-N-methylcystine

: 768-33-2
phenyldimethylsilyl chloride

: 1228275-14-6
11-methyl-8-(dimethylphenylsilyl)-7,11-diazatricyclo[7.3.1.0(2,7)]trideca-2,4-diene-6-one

: N-methyl 4-[(dimethyl)phenylsilyl]cytisine

Guidance literature:: With lithium diisopropyl amide; In tetrahydrofuran; hexane; at -78 - 20 ℃;
DOI:10.1039/c8ob01456f

Reference yield:

: 485-35-8
cytisine

: 1228275-14-6
11-methyl-8-(dimethylphenylsilyl)-7,11-diazatricyclo[7.3.1.0(2,7)]trideca-2,4-diene-6-one

Guidance literature:: Multi-step reaction with 2 steps

1: sodium cyanoborohydride / methanol; tetrahydrofuran; water / 1.5 h / 20 °C

2: N,N,N,N,-tetramethylethylenediamine; lithium diisopropyl amide / tetrahydrofuran; hexane / -78 - 20 °C

With N,N,N,N,-tetramethylethylenediamine; sodium cyanoborohydride; lithium diisopropyl amide; In tetrahydrofuran; methanol; hexane; water;
DOI:10.1039/c8ob01456f