6-ACETAMIDO-3-BROMOPYRIDINE-2-CARBOXYLIC ACID 96%6-ACETAMIDO-3-BROMOPICOLINIC ACID

Base Information

• Chemical Name: 6-ACETAMIDO-3-BROMOPYRIDINE-2-CARBOXYLIC ACID 96%6-ACETAMIDO-3-BROMOPICOLINIC ACID
• CAS No.: 882430-69-5
• Molecular Formula: C8H7BrN2O3
• Molecular Weight: 259.06
• Hs Code.: 29333990
• Mol file: 882430-69-5.mol

Synonyms:6-Acetamido-3-bromo-pyridine-2-carboxylic acid;6-Acetamido-3-bromopicolinic acid;

Chemical Property of 6-ACETAMIDO-3-BROMOPYRIDINE-2-CARBOXYLIC ACID 96%6-ACETAMIDO-3-BROMOPICOLINIC ACID

Chemical Property:

• Vapor Pressure: 2.6E-10mmHg at 25°C
• Melting Point: 196-198 °C
• Refractive Index: 1.658
• Boiling Point: 487.4 °C at 760 mmHg
• Flash Point: 248.5 °C
• PSA: 79.29000
• Density: 1.793 g/cm³
• LogP: 1.57370
• Storage Temp.: Keep Cold

Purity/Quality:

97% ^*data from raw suppliers

6-Acetylamino-3-bromo-pyridine-2-carboxylicacid ^*data from reagent suppliers

Safty Information:

• Pictogram(s): Xi
• Hazard Codes: Xi

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 6-ACETAMIDO-3-BROMOPYRIDINE-2-CARBOXYLIC ACID 96%6-ACETAMIDO-3-BROMOPICOLINIC ACID

There total 1 articles about 6-ACETAMIDO-3-BROMOPYRIDINE-2-CARBOXYLIC ACID 96%6-ACETAMIDO-3-BROMOPICOLINIC ACID which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-(5-bromo-6-methyl-pyridin-2-yl)-acetamide (142404-84-0) → 6-acetamido-3-bromopicolinic acid (882430-69-5)

Guidance literature:

With pyridine; potassium permanganate; potassium carbonate; at 90 ℃;

Reference yield:

6-acetamido-3-bromopicolinic acid (882430-69-5) + (1S,2S)-2-((4-fluorophenoxy)methyl)cyclopentan-1-amine hydrochloride → 6-acetamido-3-bromo-N-((1S,2S)-2-((4-fluorophenoxy)methyl)cyclopentyl)picolinamide

Guidance literature:

6-acetamido-3-bromopicolinic acid; (1S,2S)-2-((4-fluorophenoxy)methyl)cyclopentan-1-amine hydrochloride; In N,N-dimethyl-formamide; at 20 ℃; for 0.166667h;

With N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; In N,N-dimethyl-formamide; at 20 ℃; for 0.166667h;

With N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 20 ℃; for 16h;

Reference yield:

6-acetamido-3-bromopicolinic acid (882430-69-5) + (1S,2S)-2-((4-fluorophenoxy)methyl)cyclopentan-1-amine → 6-acetamido-3-bromo-N-((1S,2S)-2-((4-fluorophenoxy)methyl)cyclopentyl)picolinamide

Guidance literature:

With 2,4,6-tripropyl-1,3,5,2,4,6-trioxatriphosphinane-2,4,6-trioxide; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; at 20 ℃; for 16h;

upstream raw materials:

N-(5-bromo-6-methyl-pyridin-2-yl)-acetamide

Downstream raw materials:

(S)-N-(5-bromo-6-(2-(3,5-difluorophenyl)-1-(1,1-dimethylethylsulfinamido)ethyl)pyridin-2-yl)acetamide

N-(6-(1-amino-2-(3,5-difluorophenyl)ethyl)-5-bromopyridin-2-yl)acetamide hydrochloride

N-(1-(6-amino-3-bromopyridin-2-yl)-2-(3,5-difluorophenyl)ethyl)-2-(5-fluoro-1H-indol-3-yl)acetamide

5-(6-amino-2-(2-(3,5-difluorophenyl)-1-(2-(5-fluoro-1H-indol-3-yl)acetamido)ethyl)pyridin-3-yl)-2-fluorobenzamide

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