1-(tert-Butyl-diphenyl-silanyloxy)-2-methyl-2-trimethylsilanyloxy-pentan-3-one

Base Information Edit

Chemical Name:1-(tert-Butyl-diphenyl-silanyloxy)-2-methyl-2-trimethylsilanyloxy-pentan-3-one
CAS No.:118171-08-7
Molecular Formula:C₂₅H₃₈O₃Si₂
Molecular Weight:442.746
Hs Code.:
Mol file:118171-08-7.mol

Synonyms:1-(tert-Butyl-diphenyl-silanyloxy)-2-methyl-2-trimethylsilanyloxy-pentan-3-one

Suppliers and Price of 1-(tert-Butyl-diphenyl-silanyloxy)-2-methyl-2-trimethylsilanyloxy-pentan-3-one

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Chemical Property of 1-(tert-Butyl-diphenyl-silanyloxy)-2-methyl-2-trimethylsilanyloxy-pentan-3-one Edit

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Technology Process of 1-(tert-Butyl-diphenyl-silanyloxy)-2-methyl-2-trimethylsilanyloxy-pentan-3-one

There total 3 articles about 1-(tert-Butyl-diphenyl-silanyloxy)-2-methyl-2-trimethylsilanyloxy-pentan-3-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 118171-02-1
1-(tert-butyldiphenylsilyloxy)-2-propanone

: 118171-08-7
1-(tert-Butyl-diphenyl-silanyloxy)-2-methyl-2-trimethylsilanyloxy-pentan-3-one

Guidance literature:: Multi-step reaction with 2 steps

1: potassium cyanide/ 18-crown-6 / 48 h / Ambient temperature

2: diethyl ether; benzene / 48 h / Ambient temperature

With potassium cyanide; 18-crown-6 ether; In diethyl ether; benzene;
DOI:10.1021/jo00263a007

Reference yield:

: 58479-61-1
tert-butylchlorodiphenylsilane

: 118171-08-7
1-(tert-Butyl-diphenyl-silanyloxy)-2-methyl-2-trimethylsilanyloxy-pentan-3-one

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine, 4-(dimethylamino)pyridine / CH₂Cl₂ / 48 h

2: potassium cyanide/ 18-crown-6 / 48 h / Ambient temperature

3: diethyl ether; benzene / 48 h / Ambient temperature

With dmap; potassium cyanide; 18-crown-6 ether; triethylamine; In diethyl ether; dichloromethane; benzene;
DOI:10.1021/jo00263a007