5-phenyl-5-(2-tert-butoxycarbonylprop-2-enyl)-3-methylene-2-pyrrolidone

Base Information

Chemical Name:5-phenyl-5-(2-tert-butoxycarbonylprop-2-enyl)-3-methylene-2-pyrrolidone
CAS No.:1035809-90-5
Molecular Formula:C₁₉H₂₃NO₃
Molecular Weight:313.397
Hs Code.:

Synonyms:5-phenyl-5-(2-tert-butoxycarbonylprop-2-enyl)-3-methylene-2-pyrrolidone

Suppliers and Price of 5-phenyl-5-(2-tert-butoxycarbonylprop-2-enyl)-3-methylene-2-pyrrolidone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 5-phenyl-5-(2-tert-butoxycarbonylprop-2-enyl)-3-methylene-2-pyrrolidone

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 5-phenyl-5-(2-tert-butoxycarbonylprop-2-enyl)-3-methylene-2-pyrrolidone

There total 1 articles about 5-phenyl-5-(2-tert-butoxycarbonylprop-2-enyl)-3-methylene-2-pyrrolidone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 53913-96-5
tert-butyl 2-(bromomethyl)acrylate

: 100-47-0
benzonitrile

: 1035809-90-5
5-phenyl-5-(2-tert-butoxycarbonylprop-2-enyl)-3-methylene-2-pyrrolidone

Guidance literature:: With zinc; In tetrahydrofuran; for 2h; Heating;
DOI:10.1055/s-1993-26026

Reference yield: 91.0%

: 1035809-90-5
5-phenyl-5-(2-tert-butoxycarbonylprop-2-enyl)-3-methylene-2-pyrrolidone

: 5-phenyl-5-(2-carboxyprop-2-enyl)-3-methylene-2-pyrrolidinone

Guidance literature:: With hydrogenchloride; In nitromethane; 0 deg C until sat.; RT, 3 h;
DOI:10.1055/s-1993-26026

Reference yield:

: 1035809-90-5
5-phenyl-5-(2-tert-butoxycarbonylprop-2-enyl)-3-methylene-2-pyrrolidone

: 8-phenyl 2,3,5,6,7,8-hexahydro-2,6-dimethylene-1H-pyrrolizidine-3,5-dione

Guidance literature:: Multi-step reaction with 2 steps

1: 91 percent / HCl / nitromethane / 0 deg C until sat.; RT, 3 h

2: 81 percent / MsCl, Bu₄NHSO₄, E₃tN / CHCl₃ / 4 h / Ambient temperature

With hydrogenchloride; tetra(n-butyl)ammonium hydrogensulfate; methanesulfonyl chloride; triethylamine; In nitromethane; chloroform;
DOI:10.1055/s-1993-26026