C-(5-PHENYL-[1,3,4]OXADIAZOL-2-YL)-METHYLAMINE

Base Information

• Chemical Name: C-(5-PHENYL-[1,3,4]OXADIAZOL-2-YL)-METHYLAMINE
• CAS No.: 46182-58-5
• Molecular Formula: C9H9N3O
• Molecular Weight: 175.19
• Hs Code.: 2934999090
• Mol file: 46182-58-5.mol

Synonyms:3-Aminomethyl-5-phenyl-1,3,4-oxadiazole;[(5-Phenyl-1,3,4-oxadiazol-2-yl)methyl]amine;

Chemical Property of C-(5-PHENYL-[1,3,4]OXADIAZOL-2-YL)-METHYLAMINE

Chemical Property:

• Vapor Pressure: 0.000229mmHg at 25°C
• Refractive Index: 1.578
• Boiling Point: 325.5 °C at 760 mmHg
• Flash Point: 150.7 °C
• PSA: 64.94000
• Density: 1.217 g/cm³
• LogP: 1.89560
• Storage Temp.: 2-8°C

Purity/Quality:

97% ^*data from raw suppliers

(5-Phenyl-1,3,4-oxadiazol-2-yl)methanamine ^*data from reagent suppliers

Safty Information:

• Pictogram(s): Xi
• Hazard Codes: Xi,T
• Statements: 25
• Safety Statements: 45

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of C-(5-PHENYL-[1,3,4]OXADIAZOL-2-YL)-METHYLAMINE

There total 8 articles about C-(5-PHENYL-[1,3,4]OXADIAZOL-2-YL)-METHYLAMINE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 26.0%

5-phenyl-1,3,4-oxadiazole-2-carbonitrile (68496-63-9) → (5-phenyl-1,3,4-oxadiazol-2-yl)methanamine (46182-58-5)

Guidance literature:

With hydrogenchloride; hydrogen; palladium; In ethanol; water; for 2.5h;

Reference yield:

2-(azidomethyl)-5-phenyl-1,3,4-oxadiazole (934638-47-8) → (5-phenyl-1,3,4-oxadiazol-2-yl)methanamine (46182-58-5)

Guidance literature:

With palladium on activated charcoal; hydrogen; In methanol; at 20 ℃; under 3040.2 Torr;

DOI:10.1016/j.ejmech.2016.02.015

Reference yield:

C9H11N3O → (5-phenyl-1,3,4-oxadiazol-2-yl)methanamine (46182-58-5)

Guidance literature:

With trifluoroacetic acid; In dichloromethane; at 20 ℃;

DOI:10.1016/j.bmc.2021.116529

upstream raw materials:

N'-benzoyl-2-benzyloxycarbonylamino-acetohydrazonic acid ethyl ester

5-phenyl-1,3,4-oxadiazole-2-carbonitrile

benzoic acid hydrazide

2-(chloromethyl)-5-phenyl-1,3,4-oxadiazole

Downstream raw materials:

N-(5-phenyl-[1,3,4]oxadiazol-2-yl-methyl)-4-(4'-trifluoromethyl-biphenyl-2-carbonyl-amino)-1-methyl-pyrrole-2-carboxylic acid amide

2-cyanoethyl [(5-phenyl-1 ,3,4-oxadiazol-2-yl)methyl]dithiocarbamate

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