Technology Process of C17H23NO5
There total 6 articles about C17H23NO5 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
hydrogen; acetic acid;
In
methanol;
at 20 - 60 ℃;
for 7h;
DOI:10.1021/ol2009686
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / dichloromethane / 2 h / Reflux
2.1: water; acetic acid / 7 h / 20 °C
3.1: sodium periodate; silica gel / dichloromethane / 0.5 h / 20 °C
4.1: triethylamine / toluene / 2 h / Reflux
4.2: 2 h / 20 °C
5.1: 2,4,6-trimethyl-pyridine / dichloromethane / 1 h / -78 °C
6.1: potassium carbonate / methanol / 0.17 h / 20 °C
7.1: hydrogen; acetic acid / methanol / 7 h / 20 - 60 °C
With
tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; 2,4,6-trimethyl-pyridine; sodium periodate; water; hydrogen; silica gel; potassium carbonate; acetic acid; triethylamine;
In
methanol; dichloromethane; toluene;
DOI:10.1021/ol2009686
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: sodium periodate; silica gel / dichloromethane / 0.5 h / 20 °C
2.1: triethylamine / toluene / 2 h / Reflux
2.2: 2 h / 20 °C
3.1: 2,4,6-trimethyl-pyridine / dichloromethane / 1 h / -78 °C
4.1: potassium carbonate / methanol / 0.17 h / 20 °C
5.1: hydrogen; acetic acid / methanol / 7 h / 20 - 60 °C
With
2,4,6-trimethyl-pyridine; sodium periodate; hydrogen; silica gel; potassium carbonate; acetic acid; triethylamine;
In
methanol; dichloromethane; toluene;
DOI:10.1021/ol2009686
