C₁₇H₁₆O

Base Information

• Chemical Name: C₁₇H₁₆O
• CAS No.: 1361131-99-8
• Molecular Formula: C₁₇H₁₆O
• Molecular Weight: 236.313
• Mol file: 1361131-99-8.mol

Synonyms:C₁₇H₁₆O

Chemical Property of C₁₇H₁₆O

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₇H₁₆O

There total 1 articles about C₁₇H₁₆O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

3H-benzo[c][1,2]oxaborol-1-ol (5735-41-1) + trifluoromethanesulfonic acid 3,4-dihydronaphthalen-2-yl ester (143139-14-4) → C17H16O (1361131-99-8)

Guidance literature:

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; barium hydroxide octahydrate; water; In 1,4-dioxane; for 12h; Reflux;

DOI:10.1246/cl.2011.1386

Reference yield:

C17H16O (1361131-99-8) → C17H18O (1361132-00-4)

Guidance literature:

With palladium 10% on activated carbon; hydrogen; In ethyl acetate; at 20 ℃; for 7h; under 760.051 Torr;

DOI:10.1246/cl.2011.1386

Reference yield:

C17H16O (1361131-99-8) → C17H16O (1361132-01-5)

Guidance literature:

Multi-step reaction with 2 steps

1: palladium 10% on activated carbon; hydrogen / ethyl acetate / 7 h / 20 °C / 760.05 Torr

2: manganese(IV) oxide / dichloromethane / 16 h / Reflux

With manganese(IV) oxide; palladium 10% on activated carbon; hydrogen; In dichloromethane; ethyl acetate;

DOI:10.1246/cl.2011.1386

upstream raw materials:

3H-benzo[c][1,2]oxaborol-1-ol

trifluoromethanesulfonic acid 3,4-dihydronaphthalen-2-yl ester

Downstream raw materials:

C₁₇H₁₈O

C₁₇H₁₆O

1,3-dimethyl-5-(2-(1,2,3,4-tetrahydronaphthalen-2-yl)benzylidene)pyrimidine-2,4,6(1H,3H,5H)-trione

Refernces