1-(2',3'-Dihydroxy-5'-O-benzyl-β-D-erythro-pentofuranosyl)-N¹-benzylinosine

Base Information

Chemical Name:1-(2',3'-Dihydroxy-5'-O-benzyl-β-D-erythro-pentofuranosyl)-N¹-benzylinosine
CAS No.:161824-90-4
Molecular Formula:C₂₄H₂₄N₄O₅
Molecular Weight:448.478
Hs Code.:

1-(2',3'-Dihydroxy-5'-O-benzyl-β-D-erythro-pentofuranosyl)-N<sup>1</sup>-benzylinosine

Synonyms:1-(2',3'-Dihydroxy-5'-O-benzyl-β-D-erythro-pentofuranosyl)-N¹-benzylinosine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-(2',3'-Dihydroxy-5'-O-benzyl-β-D-erythro-pentofuranosyl)-N¹-benzylinosine

Chemical Property:

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Technology Process of 1-(2',3'-Dihydroxy-5'-O-benzyl-β-D-erythro-pentofuranosyl)-N¹-benzylinosine

There total 7 articles about 1-(2',3'-Dihydroxy-5'-O-benzyl-β-D-erythro-pentofuranosyl)-N¹-benzylinosine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 161824-94-8
1-(2'-O,3'-O-Cyclopentyl-5'-O-benzyl-β-D-erythro-pentofuranosyl)-N¹-benzylinosine

: 161824-90-4
1-(2',3'-Dihydroxy-5'-O-benzyl-β-D-erythro-pentofuranosyl)-N¹-benzylinosine

Guidance literature:: With trifluoroacetic acid; at 0 ℃; for 1h;
DOI:10.1021/jo00103a017

Reference yield: 95.0%

: 911430-77-8
1-benzyl-5'-O-benzyl-2',3'-O-isopropylideneinosine

: 161824-90-4
1-(2',3'-Dihydroxy-5'-O-benzyl-β-D-erythro-pentofuranosyl)-N¹-benzylinosine

Guidance literature:: With trifluoroacetic acid; at 0 - 20 ℃; for 3.33333h;
DOI:10.1021/jm0605379

Reference yield:

: 100-39-0
benzyl bromide

: 161824-90-4
1-(2',3'-Dihydroxy-5'-O-benzyl-β-D-erythro-pentofuranosyl)-N¹-benzylinosine

Guidance literature:: Multi-step reaction with 2 steps

1.1: NaH / dimethylformamide / 1 h / 20 °C

1.2: 71 percent / dimethylformamide / 1 h / 20 °C

2.1: 95 percent / aq. TFA / 3.33 h / 0 - 20 °C

With sodium hydride; trifluoroacetic acid; In N,N-dimethyl-formamide;
DOI:10.1021/jm0605379